发明授权
US5338810A Method for production of acrylate and acrylate-containing polymer
失效
生产含丙烯酸酯和含丙烯酸酯的聚合物的方法
- 专利标题: Method for production of acrylate and acrylate-containing polymer
- 专利标题(中): 生产含丙烯酸酯和含丙烯酸酯的聚合物的方法
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申请号: US27678申请日: 1993-03-08
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公开(公告)号: US5338810A公开(公告)日: 1994-08-16
- 发明人: Tadao Shimomura , Yoshio Irie , Hitoshi Takahashi , Katsuhiro Kajikawa , Jyunichi Saga , Teruaki Fujiwara , Takumi Hatsuda
- 申请人: Tadao Shimomura , Yoshio Irie , Hitoshi Takahashi , Katsuhiro Kajikawa , Jyunichi Saga , Teruaki Fujiwara , Takumi Hatsuda
- 申请人地址: JPX Osaka
- 专利权人: Nippon Shokubai Kagaku Kogyo Co., Ltd.
- 当前专利权人: Nippon Shokubai Kagaku Kogyo Co., Ltd.
- 当前专利权人地址: JPX Osaka
- 优先权: JPX63-270773 19881028
- 主分类号: C07C51/41
- IPC分类号: C07C51/41 ; C07C51/50 ; C07C57/04 ; C08F2/00 ; C08F120/06 ; C08F130/04
摘要:
A method for the production of an acrylate by the neutralization reaction of acrylic acid and a basic substance, comprising sequentially (A) a step of supplying acrylic acid and said basic substance to water thereby subjecting them to a neutralization reaction while constantly retaining the neutralization ratio of acrylic acid within the neutralization reaction system in the range of 75 to 100 mol %, (B) a step of adjusting the neutralization ratio of acrylic acid within said neutralization reaction system in the range of 100.1 to 110 mol % by supplying said basic substance to said neutralization reaction system, (C) a step of retaining the neutralization ratio of acrylic acid within said neutralization reaction system in the range of 100.1 to 110 mol % for a period in the range of 1 to 120 minutes thereby allowing the neutralization reaction product to age, and (D) a step of adjusting the neutralization ratio of acrylic acid within said neutralization reaction system in the range of 20 to 100 mol % by supplying acrylic acid to said neutralization reaction system, and a method for the production of an acrylate-containing polymer using the acrylate.
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