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US5648565A Process for the adiabatic preparation of mononitrotoluenes 失效
制备单硝基甲苯的绝热方法

Process for the adiabatic preparation of mononitrotoluenes
摘要:
Mononitrotoluenes can be prepared by intensively mixing together toluene, nitric acid, sulphuric acid and water, simultaneously or successively in their total amount, and, in the case of continuous preparation, redispersing the mixture at least twice, for which purpose a mixing energy of 1 to 40 watts per liter of the total reaction mixture, preferably 3 to 30 W/l, is employed per volume of the reactor, and, for the continuous procedure, the back mixing is substantially repressed. Adiabatic reaction conditions are maintained.
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