发明授权
- 专利标题: Process for the adiabatic preparation of mononitrotoluenes
- 专利标题(中): 制备单硝基甲苯的绝热方法
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申请号: US679323申请日: 1996-07-12
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公开(公告)号: US5648565A公开(公告)日: 1997-07-15
- 发明人: Bernd-Michael Konig , Helmut Judat , Heinz Ulrich Blank
- 申请人: Bernd-Michael Konig , Helmut Judat , Heinz Ulrich Blank
- 申请人地址: DEX Leverkusen
- 专利权人: Bayer Aktiengesellschaft
- 当前专利权人: Bayer Aktiengesellschaft
- 当前专利权人地址: DEX Leverkusen
- 优先权: DEX4404614.6 19940214; DEX4410417.0 19940325
- 主分类号: C01B17/88
- IPC分类号: C01B17/88 ; C07C201/08 ; C07C201/16 ; C07C205/06 ; C07C205/00
摘要:
Mononitrotoluenes can be prepared by intensively mixing together toluene, nitric acid, sulphuric acid and water, simultaneously or successively in their total amount, and, in the case of continuous preparation, redispersing the mixture at least twice, for which purpose a mixing energy of 1 to 40 watts per liter of the total reaction mixture, preferably 3 to 30 W/l, is employed per volume of the reactor, and, for the continuous procedure, the back mixing is substantially repressed. Adiabatic reaction conditions are maintained.
公开/授权文献
- US5127906A Non-reusable syringe 公开/授权日:1992-07-07
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