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US5969167A Method for making tris(hydroxyphenyl) compounds using ion exchange resins 失效
使用离子交换树脂制备三(羟基苯基)化合物的方法

Method for making tris(hydroxyphenyl) compounds using ion exchange resins
Abstract:
An improved method for the preparation of tris(4-hydroxyphenyl) compounds is provided. In particular, an improved method for preparing 1, 1, 1-tris(4'-hydroxyphenyl)ethane is provided which comprises heating a mixture comprising phenol and 4-hydroxy acetophenone in the presence of effective amounts of an ion exchange catalyst and a mercaptan as a copromoter such that the resulting 1, 1, 1-tris(4'-hydroxyphenyl)ethane is substantially free of various reaction impurities.
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