发明授权
- 专利标题: Process for the preparation of polyamides
- 专利标题(中): 制备聚酰胺的方法
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申请号: US81887申请日: 1998-05-19
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公开(公告)号: US6011131A公开(公告)日: 2000-01-04
- 发明人: Setsuo Sato , Hercules Peloggia , Tracy Hunt , Joerg Schwarzer , Ramiro Carielo Bueno , Roger A. Lovald
- 申请人: Setsuo Sato , Hercules Peloggia , Tracy Hunt , Joerg Schwarzer , Ramiro Carielo Bueno , Roger A. Lovald
- 申请人地址: PA Gulph Mills
- 专利权人: Henkel Corporation
- 当前专利权人: Henkel Corporation
- 当前专利权人地址: PA Gulph Mills
- 主分类号: C08G69/34
- IPC分类号: C08G69/34 ; C08G73/10 ; C08G69/26
摘要:
Process for the preparation of polyamides comprising the steps of A) reacting a soybean oil condensate obtained from the deodorization of refined soybean oil and which contains less than 30% by weight of free and esterified oleic acid based on the total weight of free and esterified fatty acids in said condensate, with a C.sub.1-4 alkanol in the presence of a zinc oxide catalyst to convert free fatty acids and fatty acid glyceride esters to fatty acid C.sub.1-4 alkyl esters;B) removing excess C.sub.1-4 alkanol, volatile reaction by-products, water, and the zinc oxide catalyst from the resulting reaction mixture;C) heating the reaction mixture from step B) under vacuum to obtain a distillate of fatty acid C.sub.1-4 alkyl esters;D) separating the distillate from step C) into a fraction containing mostly C.sub.16-18 saturated fatty acid C.sub.1-4 alkyl esters and a second fraction containing mostly C.sub.16-18 unsaturated fatty acid C.sub.1-4 alkyl esters wherein the oleic acid C.sub.1-4 alkyl ester content is less than about 35% by weight thereof;E) dimerizing said second fraction in the presence of montmorillonite clay; andF) reacting the dimerized second fraction with a polyamine.
公开/授权文献
- USD407231S Seat 公开/授权日:1999-03-30
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