发明授权
- 专利标题: Process for the preparation of phosphoric monoester
- 专利标题(中): 制备磷酸单酯的方法
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申请号: US245843申请日: 1999-02-08
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公开(公告)号: US6034261A公开(公告)日: 2000-03-07
- 发明人: Akira Matsunaga , Akira Fujiu , Shinji Tsuyutani , Toshio Nozaki , Masayuki Ueda
- 申请人: Akira Matsunaga , Akira Fujiu , Shinji Tsuyutani , Toshio Nozaki , Masayuki Ueda
- 申请人地址: JPX Tokyo
- 专利权人: Kao Corporation
- 当前专利权人: Kao Corporation
- 当前专利权人地址: JPX Tokyo
- 优先权: JPX6-306364 19941209
- 主分类号: C07F9/09
- IPC分类号: C07F9/09 ; C07F9/11
摘要:
An organic hydroxyl compound is reacted with a phosphorylating agent comprising phosphorus pentaoxide and at least one compound selected from the group consisting of water, phosphoric acid and polyphosphoric acid and having a value represented by formula (I) of from 0.5 to 1.0, under such a condition that the ratio as defined by formula (II) has a value in the range of from 2.8 to 3.2; or alternatively, an organic hydroxyl compound is reacted with the above phosphorylating agent under such a condition that the ratio as defined by formula (II) has a value in the range of from exceeding 3.2 up to 6.4 and then phosphorus pentaoxide is added to the reaction product in such an amount that the ratio as defined by formula (II) has a value in the range of from 2.8 to 3.2 with respect to the total feeds of the starting materials to conduct further reaction: ##EQU1## The above process produces a phosphoric ester mixture that is excellent in hue and odor, is reduced in the amount of orthophosphoric acid and contains a phosphoric monoester useful as a component of a detergent.
公开/授权文献
- US4899164A Slot coupled microstrip constrained lens 公开/授权日:1990-02-06