发明授权
- 专利标题: Process and unit for the production of 1,2-dichloroethane
- 专利标题(中): 用于生产1,2-二氯乙烷的方法和单元
-
申请号: US09549682申请日: 2000-04-14
-
公开(公告)号: US06252125B1公开(公告)日: 2001-06-26
- 发明人: Peter Porscha
- 申请人: Peter Porscha
- 优先权: DE19916753 19990414
- 主分类号: C07C1702
- IPC分类号: C07C1702
摘要:
By a process for the production of 1,2-dichloroethane (EDC) by reaction of ethylene with chlorine in the liquid phase (direct chlorination), the heavy ends being separated from the obtained 1,2-dichloroethane in a heavy-ends column and in a downstream vacuum column and, for the purpose of heat recovery and heating of the column bottoms, a 1,2-dichloroethane part-stream from the direct chlorination passing through a heat exchanger (one attributed to each column) for indirect heat exchange with the bottom product of each column, the aim of the invention is to provide a solution in which the reaction enthalpy of the direct chlorination can be used in a variable manner, thus precluding the above-described disadvantages. This is achieved by using at least one falling-film evaporator for heating the column bottoms, the bottom product of the respective column being routed to the distributor at the head of the column.
信息查询