公开(公告)号：US07959768B2

公开(公告)日：2011-06-14

申请号：US11662461

申请日：2005-09-13

申请人： Peter Porscha ,  Michael Benje ,  Harald Hafenscher

发明人： Peter Porscha ,  Michael Benje ,  Harald Hafenscher

IPC分类号： B01D1/06 ,  B01D3/28 ,  B01D3/42

CPC分类号： B01D1/065 ,  Y02P70/34 ,  Y10S203/07 ,  Y10S203/11

摘要： The invention relates to a falling film evaporator, which is fitted with a liquid distributor which is divided into segments, such that it is possible to charge only a limited number of evaporator tubes with liquid and the evaporator can be operated in an optimum manner even with a partial load. The invention also relates to a method for operating said falling film evaporator, the aim of which is to transfer heat, which is released when a gas-vapor mixture is condensed, to a liquid which is to be evaporated at least partially. It would be useful to use said falling film evaporator thus fitted in heat recuperation systems such as those used in the production of 1,2 dichloroethane.

摘要翻译： 本发明涉及一种降膜蒸发器，其装配有被分成段的液体分配器，使得可以仅使用有限数量的具有液体的蒸发器管进行充​​气，并且蒸发器可以以最佳方式操作，即使 部分负载。 本发明还涉及一种用于操作所述降膜蒸发器的方法，其目的是将气体 - 蒸汽混合物冷凝时释放的热量传递至至少部分蒸发的液体。 使用这样安装在热回收系统（如用于生产1,2-二氯乙烷的那些）中的降膜蒸发器将是有用的。

公开(公告)号：US20070272298A1

公开(公告)日：2007-11-29

申请号：US10571247

申请日：2004-09-10

申请人： Peter Porscha

发明人： Peter Porscha

IPC分类号： F17D1/08

CPC分类号： B01D53/185 ,  B01D3/008 ,  B01J8/065 ,  Y10T137/0318 ,  Y10T137/4807

摘要： A liquid distributor for two liquid phases to be uniformly distributed into a plurality of tubes of an upright tube-bundle reactor for carrying out chemical reactions, wherein the inside of the tubes forming the tube bundle are provided for a trickle-bed operation, the tubes are retained at the top and bottom by tubesheets and are closed against the outside of the tube, a distribution chamber is arranged above the upper tubesheet, which chamber contains feed pipes for two different liquids and at least one gas phase, wherein a first liquid distribution system is arranged directly above the tubesheet or on it, which system is connected to at least one outer feed device and contains an annular weir installed outside the tubed area, with openings at the bottom and a plurality of inlet sleeves, wherein one inlet sleeve is assigned at the top to each of the tubes of the tube bundle, the inlet sleeves are of tubular design and are vertically aligned, and the said sleeves have at least one lateral and one further opening located above the tubesheet and are open at the bottom facing each assigned tube in the tube bundle, and wherein a second liquid distribution system is arranged above the first liquid distribution system, which system is connected to at least one other outer feed device and contains one upper and one lower distribution tray, wherein the lower distribution tray contains a plurality of openings which are arranged flush above the inlet sleeves of the first liquid distribution system, and exhibits at least one device for setting a uniform liquid level above the openings, wherein the upper distribution tray is connected to the feed device for liquid, and contains a plurality of overflow weirs from which the liquid is able to discharge into the lower distribution tray, and wherein each of the overflow weirs is assigned to a plurality of openings of the lower distribution tray.

摘要翻译： 用于两个液相的液体分配器被均匀分布到用于进行化学反应的直立管束反应器的多个管中，其中形成管束的管的内部设置用于滴流床操作，管 通过管板被保持在顶部和底部并且被封闭抵靠管的外部，分配室布置在上管板上方，该室包含用于两种不同液体的进料管和至少一个气相，其中第一液体分布 系统直接布置在管板的上方或其上，该系统连接到至少一个外部进料装置，并且包含安装在管状区域外部的环形堰，在底部具有开口并具有多个入口套筒，其中一个入口套筒是 分配在管束的每个管的顶部，入口套筒为管状设计并且垂直对准，并且所述套筒具有至少一个1a 并且在底部处朝向管束中的每个分配的管开口，并且其中第二液体分配系统布置在第一液体分配系统的上方，该系统连接到至少一个其它外部 进料装置，并且包含一个上部和一个下部分配托盘，其中下部分配托盘包含多个开口，其布置成齐平在第一液体分配系统的入口套筒上方，并且具有至少一个用于设定上述均匀液面的装置 开口，其中上部分配托盘连接到用于液体的进料装置，并且包含多个溢流堰，液体能够从该溢流堰排出到下分配塔板中，并且其中每个溢流堰分配给多个 下部分配托盘的开口。

公开(公告)号：US07182840B1

公开(公告)日：2007-02-27

申请号：US10129344

申请日：2000-10-28

申请人： Michael Benje ,  Peter Porscha ,  Stefan Von Egelstein

发明人： Michael Benje ,  Peter Porscha ,  Stefan Von Egelstein

IPC分类号： B01D3/28 ,  C07C17/383

CPC分类号： C07C17/02 ,  Y02P20/582 ,  Y10S203/08 ,  Y10S203/09 ,  C07C19/045

摘要： The invention relates to a method and a device for the optimal use of reaction heat resulting from the production of 1,2-dichloroethane from ethene and chlorine. The aim of the invention is achieved by extracting reaction heat liberated during the reaction of chlorine with ethene and the reaction heat contained in 1,2-dichloroethane. Extraction of said reaction heat from the reaction chamber occurs using at least one part of gaseous 1,2-dichloroethane (latent heat) and at least one part of liquid 1,2-dichloroethane (feelable heat) removed from the reaction chamber. Said reaction heat is used to heat two fractioning columns in order to purify 1,2-dichloroethane of impurities having a boiling point higher than 1,2-dichloroethane.

摘要翻译： 本发明涉及一种用于从乙烯和氯生产1,2-二氯乙烷产生的反应热的最佳使用的方法和装置。 本发明的目的是通过提取在氯与乙烯的反应期间释放的反应热和1,2-二氯乙烷中所含的反应热来实现。 使用至少一部分气态1,2-二氯乙烷（潜热）和从反应室中除去至少一部分液体1,2-二氯乙烷（感觉热），从反应室中提取所述反应热。 所述反应热用于加热两个分馏塔，以便纯化1,2-二氯乙烷的沸点高于1,2-二氯乙烷的杂质。

公开(公告)号：US07670572B2

公开(公告)日：2010-03-02

申请号：US10571247

申请日：2004-09-10

申请人： Peter Porscha

发明人： Peter Porscha

IPC分类号： B01J10/00

CPC分类号： B01D53/185 ,  B01D3/008 ,  B01J8/065 ,  Y10T137/0318 ,  Y10T137/4807

摘要： A distributor includes first and second liquid distribution systems for two liquid phases for an upright tube-bundle reactor. The first system is arranged directly above or on a tubesheet and is connected to at least one outer feed device and contains an annular weir. The second system is connected to at least one other outer feed device and contains one upper and one lower distribution tray which contains a plurality of openings which are arranged flush above the inlet sleeves of the first system, and has at least one device for setting a uniform liquid level above the openings. The upper distribution tray is connected to the feed device for liquid, and contains a plurality of overflow weirs from which the liquid is able to discharge into the lower distribution tray. Each of the overflow weirs is assigned to a plurality of openings of the lower distribution tray.

摘要翻译： 分配器包括用于直立管束反应器的两个液相的第一和第二液体分配系统。 第一系统直接布置在管板的上方或上方，并连接到至少一个外部进料装置并且包含环形堰。 第二系统连接到至少一个其它外部进料装置，并且包含一个上部分配塔板和一个下部分配托盘，该分配托盘包含多个开口，该多个开口布置在第一系统的入口套筒的上方，并且具有至少一个用于设置 均匀的液面高于开口。 上部分配托盘连接到用于液体的进料装置，并且包含多个溢流堰，液体能从该溢流堰排出到下部分配塔板中。 每个溢流堰被分配给下分配盘的多个开口。

公开(公告)号：US20080196839A1

公开(公告)日：2008-08-21

申请号：US11662461

申请日：2005-09-13

申请人： Peter Porscha ,  Michael Benje ,  Harald Hafenscher

发明人： Peter Porscha ,  Michael Benje ,  Harald Hafenscher

IPC分类号： B01D1/06

CPC分类号： B01D1/065 ,  Y02P70/34 ,  Y10S203/07 ,  Y10S203/11

摘要： The invention relates to a falling film evaporator, which is fitted with a liquid distributor which is divided into segments, such that it is possible to charge only a limited number of evaporator tubes with liquid and the evaporator can be operated in an optimum manner even with a partial load. The invention also relates to a method for operating said falling film evaporator, the aim of which is to transfer heat, which is released when a gas-vapor mixture is condensed, to a liquid which is to be evaporated at least partially. It would be useful to use said falling film evaporator thus fitted in heat recuperation systems such as those used in the production of 1,2 dichloroethane.

摘要翻译： 本发明涉及一种降膜蒸发器，其装配有被分成段的液体分配器，使得可以仅使用有限数量的具有液体的蒸发器管进行充​​气，并且蒸发器可以以最佳方式操作，即使 部分负载。 本发明还涉及一种用于操作所述降膜蒸发器的方法，其目的是将气体 - 蒸汽混合物冷凝时释放的热量传递至至少部分蒸发的液体。 使用这样安装在热回收系统（如用于生产1,2-二氯乙烷的那些）中的降膜蒸发器将是有用的。

公开(公告)号：US06252125B1

公开(公告)日：2001-06-26

申请号：US09549682

申请日：2000-04-14

申请人： Peter Porscha

发明人： Peter Porscha

IPC分类号： C07C1702

CPC分类号： C07C17/02 ,  C07C17/383 ,  Y02P20/124 ,  Y02P20/51 ,  C07C19/045

摘要： By a process for the production of 1,2-dichloroethane (EDC) by reaction of ethylene with chlorine in the liquid phase (direct chlorination), the heavy ends being separated from the obtained 1,2-dichloroethane in a heavy-ends column and in a downstream vacuum column and, for the purpose of heat recovery and heating of the column bottoms, a 1,2-dichloroethane part-stream from the direct chlorination passing through a heat exchanger (one attributed to each column) for indirect heat exchange with the bottom product of each column, the aim of the invention is to provide a solution in which the reaction enthalpy of the direct chlorination can be used in a variable manner, thus precluding the above-described disadvantages. This is achieved by using at least one falling-film evaporator for heating the column bottoms, the bottom product of the respective column being routed to the distributor at the head of the column.

摘要翻译： 通过在液相（直接氯化）中通过乙烯与氯的反应生产1,2-二氯乙烷（EDC）的方法，将重质末端与重馏分塔中的所得1,2-二氯乙烷分离， 在下游真空塔中，为了塔底的热回收和加热，从直接氯化的1,2-二氯乙烷部分物流通过热交换器（一个归因于每个塔），用于与 每列的底部产物，本发明的目的是提供一种溶液，其中可以以可变的方式使用直接氯化的反应焓，从而排除上述缺点。这通过使用至少一种 用于加热柱底的降膜蒸发器，相应塔的底部产物被引导到塔顶部的分配器。