发明授权
US06706346B2 Process for production of metal encased polyimide molded bodies and metal encased polyimide molded bodies
有权
金属包覆的聚酰亚胺成型体和金属包覆的聚酰亚胺成型体的制造方法
- 专利标题: Process for production of metal encased polyimide molded bodies and metal encased polyimide molded bodies
- 专利标题(中): 金属包覆的聚酰亚胺成型体和金属包覆的聚酰亚胺成型体的制造方法
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申请号: US09909834申请日: 2001-07-23
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公开(公告)号: US06706346B2公开(公告)日: 2004-03-16
- 发明人: Tatsuo Tsumiyama
- 申请人: Tatsuo Tsumiyama
- 优先权: JP2000-221996 20000724
- 主分类号: B29D3100
- IPC分类号: B29D3100
摘要:
A process for production of polyimide molded bodies which comprises a step in which a polyimide resin powder obtained by polymerization and imidation of p-phenylenediamine with 3,3,4,4′-biphenyltetracarboxylic acid, its ester or its dianhydride and 2,3,3′,4′-biphenyltetracarboxylic acid, its ester or its dianhydride is molded at a pressure of approximately 800-5,000 kgf/cm2, a step in which the pressurized body is subjected to calcination at about 450-550° C. under low pressure, a step in which the calcined molded body is vacuum encapsulated into a metal capsule, and a step in which the encapsulated molded body is isotropically subjected to hot compression at approximately 460-550° C. in an inert gas atmosphere such as argon. The polyimide molded bodies obtained thereby have a density in the range of 1.44-1.38 g/cm3.
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