发明授权
- 专利标题: Column packing material and method for producing the same
- 专利标题(中): 柱填料及其制造方法
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申请号: US10398564申请日: 2002-08-30
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公开(公告)号: US07329386B2公开(公告)日: 2008-02-12
- 发明人: Atsushi Kobayashi , Kazuko Takezawa , Hideki Takasaki , Taketoshi Kanda , Isao Tanaka , Tomoko Kimura , Yutaka Ohtsu
- 申请人: Atsushi Kobayashi , Kazuko Takezawa , Hideki Takasaki , Taketoshi Kanda , Isao Tanaka , Tomoko Kimura , Yutaka Ohtsu
- 申请人地址: JP Tokyo
- 专利权人: Shiseido Co., Ltd.
- 当前专利权人: Shiseido Co., Ltd.
- 当前专利权人地址: JP Tokyo
- 代理机构: Andrews Kurth LLP
- 代理商 Fei-fei Chao
- 国际申请: PCT/JP02/08782 WO 20020830
- 国际公布: WO03/019177 WO 20030306
- 主分类号: G01N30/56
- IPC分类号: G01N30/56
摘要:
The first subject of this invention is a column packing material comprising: a silica gel having a silanol group; a first chemical modification group which is bound to said silanol group; a silicone polymer for coating the surface of said silica gel; and, a trimethylsilyl group which is bound to the silanol group on said silicone polymer and/or the silanol group on said silica gel. The second subject of this invention is a method for producing a column packing material comprising the following steps (A) to (C): (A) a step for introducing a first chemical modification group into a silanol group on the surface of a silica gel by reacting the silica gel with a silane coupling agent having said first chemical modification group; (B) a step for forming a silicone polymer coating on the surface of said silica gel by polymerizing one or more silicone compounds on the surface of the silica gel after step (A); and, (C) a step for trimethylsilylating a silanol group on said silicone polymer and/or a silanol group on said silica gel using an end-capping agent after step (B).
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