发明授权
- 专利标题: Hydroxymethyl furfural oxidation methods
- 专利标题(中): 羟甲基糠醛氧化法
-
申请号: US11932436申请日: 2007-10-31
-
公开(公告)号: US07700788B2公开(公告)日: 2010-04-20
- 发明人: Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
- 申请人: Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
- 申请人地址: US WA Richland
- 专利权人: Battelle Memorial Institute
- 当前专利权人: Battelle Memorial Institute
- 当前专利权人地址: US WA Richland
- 代理机构: Wells St. John P.S.
- 主分类号: C07D307/44
- IPC分类号: C07D307/44
摘要:
A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50° C. to about 200° C. A method of producing an oxidation catalyst where ZrO2 is provided and is calcined. The ZrO2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O2.
公开/授权文献
- US20080103318A1 Hydroxymethyl Furfural Oxidation Methods 公开/授权日:2008-05-01