发明授权
US08529651B2 Process for the production of metal oxide and metalloid oxide dispersions
有权
用于生产金属氧化物和类金属氧化物分散体的方法
- 专利标题: Process for the production of metal oxide and metalloid oxide dispersions
- 专利标题(中): 用于生产金属氧化物和类金属氧化物分散体的方法
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申请号: US12894539申请日: 2010-09-30
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公开(公告)号: US08529651B2公开(公告)日: 2013-09-10
- 发明人: Wolfgang Lortz , Christoph Batz-Sohn , Gabriele Perlet , Werner Will , Gerrit Schneider
- 申请人: Wolfgang Lortz , Christoph Batz-Sohn , Gabriele Perlet , Werner Will , Gerrit Schneider
- 申请人地址: DE Essen
- 专利权人: Evonik Degussa GmbH
- 当前专利权人: Evonik Degussa GmbH
- 当前专利权人地址: DE Essen
- 代理机构: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- 优先权: DE10317066 20030414
- 主分类号: B24D3/02
- IPC分类号: B24D3/02 ; C09C1/68 ; C09K3/14 ; C01B33/12
摘要:
Process for the production of an aqueous dispersion of pyrogenically produced metal oxide and metalloid oxide powders with a BET surface area of between 5 and 600 m2/g, with a metal oxide or metalloid oxide content in the dispersion of between 5 and 25 wt. %, comprising the following steps: water, which is optionally adjusted to pH values of between 2 and 4 by adding acids, is circulated from a receiving vessel via a rotor/stator machine, and metal oxide or metalloid oxide powder is introduced, using a feed device, into the shear zone between the slots in the rotor teeth and the stator slots, continuously or discontinuously and with the rotor/stator machine running, in a quantity such that a predispersion with a solids content of between 20 and 40 wt. % results, and, after all the metal oxide powder or metalloid oxide powder has been added, the feed device closes and shearing continues in such a way that the shear rate is in the range of between 10000 and 40000 s−1, and then, by dilution, the predispersion is adjusted to the desired solids content of the dispersion while maintaining the dispersing conditions.
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