Invention Grant
US08609899B2 Process for preparing toluenediamine by hydrogenation of dinitrotoluene
有权
通过氢化二硝基甲苯制备甲苯二胺的方法
- Patent Title: Process for preparing toluenediamine by hydrogenation of dinitrotoluene
- Patent Title (中): 通过氢化二硝基甲苯制备甲苯二胺的方法
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Application No.: US13109399Application Date: 2011-05-17
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Publication No.: US08609899B2Publication Date: 2013-12-17
- Inventor: Andreas Raichle , Joana Coelho Tsou , Samuel Neto , Ulrich Penzel , Steffen Oehlenschlaeger , Michael Zoellinger , Holgar Braunsberg , Stefanie Haase , Johannes Buettner
- Applicant: Andreas Raichle , Joana Coelho Tsou , Samuel Neto , Ulrich Penzel , Steffen Oehlenschlaeger , Michael Zoellinger , Holgar Braunsberg , Stefanie Haase , Johannes Buettner
- Applicant Address: DE Ludwigshafen
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen
- Agency: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- Main IPC: C07C209/00
- IPC: C07C209/00

Abstract:
The invention relates to a process for the continuous preparation of toluenediamine by liquid-phase hydrogenation of dinitrotoluene by means of hydrogen in the presence of a suspended, nickel-comprising catalyst in a reactor with a product isolation unit downstream of the reactor to give a product output from the reactor comprising a liquid phase comprising toluenediamine and dinitrotoluene, in which the nickel-comprising catalyst is suspended, wherein the concentration of dinitrotoluene in the liquid phase of the product output from the reactor in the region between the reactor and the downstream product isolation unit is set to a value in the range from 1 to 200 ppm by weight, based on the total weight of the liquid phase of the product output from the reactor.
Public/Granted literature
- US20110295039A1 PROCESS FOR PREPARING TOLUENEDIAMINE BY HYDROGENATION OF DINITROTOLUENE Public/Granted day:2011-12-01
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