发明授权
- 专利标题: Process for producing monosilane from dichlorosilane
- 专利标题(中): 二氯硅烷生产甲硅烷的方法
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申请号: US13820450申请日: 2011-08-29
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公开(公告)号: US08871168B2公开(公告)日: 2014-10-28
- 发明人: Isao Abe , Jérôme Beauvisage , Shinji Tomita
- 申请人: Isao Abe , Jérôme Beauvisage , Shinji Tomita
- 申请人地址: FR Paris
- 专利权人: L'Air Liquide, Societe Anonyme pour l'Etude et l'Exploitation des Procedes Georges Claude
- 当前专利权人: L'Air Liquide, Societe Anonyme pour l'Etude et l'Exploitation des Procedes Georges Claude
- 当前专利权人地址: FR Paris
- 代理商 Allen E. White
- 优先权: EP10305946 20100903
- 国际申请: PCT/EP2011/064798 WO 20110829
- 国际公布: WO2012/028571 WO 20120308
- 主分类号: C01B33/04
- IPC分类号: C01B33/04 ; B01J31/02
摘要:
A process for continuously producing monosilane by means of an apparatus comprising a reaction column, at least two upper condensers each with a reflux feed pipe, a bottom reboiler and an evaporation tank connected to a bottom portion of the reaction column; the process comprising: a) supplying dichlorosilane or a mixture of chlorosilanes to an upper stage of the reaction column via an upper feed injection point b) supplying a catalyst to said upper stage of the reaction column via a lower injection point c) introducing the resultant mixture from the top portion of the reaction column to the plurality of upper condensers d) separating monosilane from condensates in the upper condensers e) recycling the condensates through the reflux feed pipes to the upper stage of the reaction column f) bringing the condensates into contact with the catalyst in the reaction column.
公开/授权文献
- US20130272948A1 PROCESS FOR PRODUCING MONOSILANE FROM DICHLOROSILANE 公开/授权日:2013-10-17
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