Invention Grant
- Patent Title: Preparation of diamine via the preparation of aminonitrile
- Patent Title (中): 通过制备氨基腈制备二胺
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Application No.: US13982694Application Date: 2012-02-03
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Publication No.: US09079823B2Publication Date: 2015-07-14
- Inventor: Philippe Leconte
- Applicant: Philippe Leconte
- Applicant Address: FR Aubervilliers
- Assignee: RHODIA OPERATIONS
- Current Assignee: RHODIA OPERATIONS
- Current Assignee Address: FR Aubervilliers
- Agent Xuping Fu
- Priority: FR1150908 20110204
- International Application: PCT/EP2012/051882 WO 20120203
- International Announcement: WO2012/104420 WO 20120809
- Main IPC: C07C209/48
- IPC: C07C209/48 ; C07C253/30

Abstract:
A continuous method (P) for preparing diamine is described. The method includes reacting the corresponding alkene nitrile with the corresponding monoamine in order to form the corresponding aminonitrile. The monoamine can be introduced in molecular excess with respect to the alkene nitrile, wherein the unreacted monoamine is recirculated to the reaction; followed by reducing the aminonitrile produced by hydrogen in the presence of at least one alkali-metal hydroxide, water, and a hydrogenation catalyst; and purifying the diamine.
Public/Granted literature
- US20140012045A1 PREPARATION OF DIAMINE VIA THE PREPARATION OF AMINONITRILE Public/Granted day:2014-01-09
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