发明授权
- 专利标题: Liquid-liquid separator interface detection system and polymerization process utilizing the same
- 专利标题(中): 液 - 液分离器界面检测系统及其使用的聚合方法
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申请号: US14391178申请日: 2013-03-14
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公开(公告)号: US09327221B2公开(公告)日: 2016-05-03
- 发明人: Curvel Hypolite , Alec Y. Wang
- 申请人: Dow Global Technologies LLC
- 申请人地址: US MI Midland
- 专利权人: Dow Global Technologies LLC
- 当前专利权人: Dow Global Technologies LLC
- 当前专利权人地址: US MI Midland
- 国际申请: PCT/US2013/031163 WO 20130314
- 国际公布: WO2013/169357 WO 20131114
- 主分类号: C08F6/12
- IPC分类号: C08F6/12 ; C08F2/04 ; B01D35/157 ; G01N29/024 ; C08F210/18 ; G01N29/22 ; C08F210/16 ; G01F23/296
摘要:
A system for detecting an interface between a polymer-rich phase and a solvent-rich phase comprising a liquid-liquid separator configured to receive a polymer solution as an inlet stream comprising solvent, polymer and unreacted monomer produced in a solvent-based polymerization reactor through an inlet feed, wherein a tank is configured to provide a residence time of at least 20 minutes and to permit the stream to separate into the polymer rich phase and the solvent rich phase; a first sonic transponder for sending a first sonic signal from either a top or bottom of the liquid-liquid separator and for receiving a first reflected portion of the sonic signal, the reflected portion of the sonic signal created by the passage of the sonic signal through a liquid-liquid interface between the solvent rich phase and the polymer rich phase, wherein the first sonic transponder is positioned such that it transmits the signal which travels perpendicularly to the liquid-liquid interface is provided.
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