发明授权
US09475761B2 Method for producing cyanogen-halide, cyanate ester compound and method for producing the same, and resin composition
有权
氰卤化物,氰酸酯化合物的制造方法及其制造方法以及树脂组合物
- 专利标题: Method for producing cyanogen-halide, cyanate ester compound and method for producing the same, and resin composition
- 专利标题(中): 氰卤化物,氰酸酯化合物的制造方法及其制造方法以及树脂组合物
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申请号: US14436295申请日: 2013-10-25
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公开(公告)号: US09475761B2公开(公告)日: 2016-10-25
- 发明人: Masayuki Katagiri , Yuuichi Sugano , Taketo Ikeno , Makoto Tsubuku , Keita Tokuzumi , Kenj Arii , Takashi Kobayashi , Masanobu Sogame , Yoshinori Mabuchi , Yoshihiro Kato
- 申请人: MITSUBISHI GAS CHEMICAL COMPANY, INC.
- 申请人地址: JP Tokyo
- 专利权人: MITSUBISHI GAS CHEMICAL COMPANY, INC.
- 当前专利权人: MITSUBISHI GAS CHEMICAL COMPANY, INC.
- 当前专利权人地址: JP Tokyo
- 代理机构: Greenblum & Bernstein, P.L.C.
- 优先权: JP2012-236302 20121026; JP2013-001002 20130108; JP2013-041491 20130304; JP2013-059992 20130322
- 国际申请: PCT/JP2013/079048 WO 20131025
- 国际公布: WO2014/065422 WO 20140501
- 主分类号: C01C3/08
- IPC分类号: C01C3/08 ; C07C261/00 ; C07C261/02 ; C01C3/00 ; B32B15/09 ; B32B27/36 ; C08G8/28 ; C08G65/48 ; C08J5/04 ; C08J5/24 ; C08L61/14 ; C08L71/00 ; C09J161/14 ; C09J171/00 ; C09K3/10 ; H05K1/03
摘要:
A method for efficiently producing a cyanogen halide with suppressed side effects, and a method for producing a high-purity cyanate ester compound at a high yield includes contacting a halogen molecule with an aqueous solution containing hydrogen cyanide and/or a metal cyanide, so that the hydrogen cyanide and/or the metal cyanide is allowed to react with the halogen molecule in the reaction solution to obtain the cyanogen halide, wherein more than 1 mole of the hydrogen cyanide or the metal cyanide is used based on 1 mole of the halogen molecule, and when an amount of substance of an unreacted hydrogen cyanide or an unreacted metal cyanide is defined as mole (A) and an amount of substance of the generated cyanogen halide is defined as mole (B), the reaction is terminated in a state in which (A):(A)+(B) is between 0.00009:1 and 0.2:1.
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