Invention Grant
US09550672B2 Method for preparation of an alane-etherate complex and alane 有权
丙烷 - 乙醚络合物和丙烷的制备方法

Method for preparation of an alane-etherate complex and alane
Abstract:
The invention relates to methods of forming an alane-etherate complex and α-alane from the alane-etherate complex. The methods include reacting an alkyl halide with a metal alanate in a solvent including an ether. A tertiary amine may also be added to the reaction. The alane is collected after removal of the solvent and/or the tertiary amine. An electrospraying process can be used to remove the solvent.
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