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公开(公告)号：US20150093579A1
公开(公告)日：2015-04-02
申请号：US14558569
申请日：2014-12-02
发明人： Allison M. Fisher
CPC分类号： C01B6/06 , C01B6/34 , Y10T428/2982
摘要： The invention to preparing alane-etherate and alane by producing an alane-etherate complex using an acid including one or a combination of hydrochloric acid and methanesulfonic acid and a metal tetrahydroaluminate in a solvent including an ether such as diethyl ether. The alane-etherate can be desolvated using a spray desolvation process such as electrospraying.
摘要翻译： 本发明通过使用包括盐酸和甲磺酸中的一种或其组合的酸和四氢铝酸金属在包括醚如乙醚的溶剂中制备丙烯 - 乙醚合物来制备烷基醚合物和丙烷。 可以使用喷雾去溶剂化方法（如电喷雾）将乙醚 - 乙醚合物脱溶剂。
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公开(公告)号：US08916305B2
公开(公告)日：2014-12-23
申请号：US14301960
申请日：2014-06-11
发明人： Richard A. Langan , Jason L. Stimits , Chad E. Law , Russell H. Barton , Thomas J. Kmetich , Allison M. Fisher , Guanghong Zheng , Olen Vanderleeden
CPC分类号： H01M8/0643 , C01B3/0005 , C01B3/0084 , C01B3/02 , C01B3/04 , C01B3/08 , C01B2203/085 , C01B2203/1619 , C01B2203/1623 , F17C11/005 , H01M8/04208 , H01M8/04216 , H01M8/0618 , H01M8/065 , Y02E60/321 , Y02E60/324 , Y02E60/327 , Y02E60/364 , Y02E60/50
摘要： Methods for generating hydrogen gas and power and related systems, including a hydrogen generator and a fuel cell system. The hydrogen generator includes a cartridge, a housing with a cavity to removably contain the cartridge, and an initiation system. The cartridge includes a casing; a plurality of pellets including a hydrogen containing material; a plurality of solid heat transfer members in contact with but not penetrating the casing; a hydrogen outlet in the casing; and a hydrogen flow path from each pellet to the hydrogen outlet. A plurality of heating elements is disposed inside the housing. Each heating element is disposed so heat can be conducted from the heating element through the casing to corresponding heat transfer member to initiate the release of hydrogen gas. The initiation system can selectively heat one or more pellets. Hydrogen gas can be provided to a fuel cell battery to generate power.
摘要翻译： 用于产生氢气和电力及相关系统的方法，包括氢发生器和燃料电池系统。 氢气发生器包括筒，具有可移除地容纳盒的空腔的壳体和起始系统。 盒包括壳体; 包含含氢材料的多个粒料; 多个固体传热构件，其与壳体接触但不穿透壳体; 壳体中的氢出口; 以及从每个颗粒到氢气出口的氢气流动路径。 多个加热元件设置在壳体内。 每个加热元件设置成使得热量可以从加热元件通过壳体传导到相应的传热元件以引发氢气的释放。 起始系统可以选择性地加热一个或多个粒料。 可以向燃料电池电池提供氢气以产生电力。
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3.发明申请公开(公告)号：US20150093325A1
公开(公告)日：2015-04-02
申请号：US14558240
申请日：2014-12-02
发明人： Allison M. Fisher
IPC分类号： C01B6/06
CPC分类号： C01B6/06
摘要： The invention relates to methods of forming an alane-etherate complex and α-alane from the alane-etherate complex. The methods include reacting an alkyl halide with a metal alanate in a solvent including an ether. A tertiary amine may also be added to the reaction. The alane is collected after removal of the solvent and/or the tertiary amine. An electrospraying process can be used to remove the solvent.
摘要翻译： 本发明涉及从丙烷 - 乙醚合物络合物形成丙烷 - 乙醚合物络合物和α-甲烷的方法。 所述方法包括使烷基卤与金属铝酸盐在包括醚的溶剂中反应。 也可以向反应中加入叔胺。 在除去溶剂和/或叔胺之后收集丙烷。 可以使用电喷雾方法除去溶剂。
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公开(公告)号：US09543604B2
公开(公告)日：2017-01-10
申请号：US14975485
申请日：2015-12-18
发明人： Richard A. Langan , Jason L. Stimits , Chad E. Law , Russell H. Barton , Thomas J. Kmetich , Allison M. Fisher , Guanghong Zheng , Olen Vanderleeden
CPC分类号： H01M8/0643 , C01B3/0005 , C01B3/0084 , C01B3/02 , C01B3/04 , C01B3/08 , C01B2203/085 , C01B2203/1619 , C01B2203/1623 , F17C11/005 , H01M8/04208 , H01M8/04216 , H01M8/0618 , H01M8/065 , Y02E60/321 , Y02E60/324 , Y02E60/327 , Y02E60/364 , Y02E60/50
摘要： A hydrogen generator and a fuel cell system including a fuel cell battery and the hydrogen generator. The hydrogen generator includes a cartridge, a housing with a cavity to removably contain the cartridge, and an initiation system. The cartridge includes a casing; a plurality of pellets including a hydrogen containing material; a plurality of solid heat transfer members in contact with but not penetrating the casing; a hydrogen outlet in the casing; and a hydrogen flow path from each pellet to the hydrogen outlet. A plurality of heating elements is disposed inside the housing. When the cartridge is in the cavity, each heating element is disposed so heat can be conducted from the heating element and through the casing and corresponding heat transfer member to initiate the release of hydrogen gas. The initiation system can selectively heat one or more pellets to release hydrogen gas as needed.
摘要翻译： 一种氢发生器和包括燃料电池和氢发生器的燃料电池系统。 氢气发生器包括筒，具有可移除地容纳盒的空腔的壳体和起始系统。 盒包括壳体; 包含含氢材料的多个粒料; 多个固体传热构件，其与壳体接触但不穿透壳体; 壳体中的氢出口; 以及从每个颗粒到氢气出口的氢气流动路径。 多个加热元件设置在壳体内。 当盒位于空腔中时，每个加热元件被设置成使得热量可以从加热元件通过壳体和相应的传热构件传导以开始释放氢气。 起始系统可以根据需要选择性地加热一个或多个粒料以释放氢气。
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5.发明申请METHOD FOR PREPARATION OF CRYSTALLINE ALANE USING QUARTERNARY AMMONIUM ALUMINUM HYDRIDE 审中-公开使用季铵金属氢氧化物制备结晶橙的方法公开(公告)号：US20150210543A1
公开(公告)日：2015-07-30
申请号：US14678303
申请日：2015-04-03
发明人： Allison M. Fisher
IPC分类号： C01B6/06
CPC分类号： C01B6/06
摘要： The invention relates to a method of forming α-alane. The method includes reacting a tetraalkyl ammonium alanate solution in toluene with an alkyl halide or other proton source such as HCl or H2SO4.
摘要翻译： 本发明涉及一种形成α-烯烃的方法。 该方法包括使甲烷中的四烷基铵铝酸盐溶液与烷基卤化物或其它质子源如HCl或H 2 SO 4反应。
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公开(公告)号：US20150023846A1
公开(公告)日：2015-01-22
申请号：US14506260
申请日：2014-10-03
发明人： Richard A. Langan , Jason L. Stimits , Chad E. Law , Russell H. Barton , Thomas J. Kmetich , Allison M. Fisher , Guanghong Zheng , Olen Vanderleeden
IPC分类号： H01M8/06
CPC分类号： H01M8/0643 , C01B3/0005 , C01B3/0084 , C01B3/02 , C01B3/04 , C01B3/08 , C01B2203/085 , C01B2203/1619 , C01B2203/1623 , F17C11/005 , H01M8/04208 , H01M8/04216 , H01M8/0618 , H01M8/065 , Y02E60/321 , Y02E60/324 , Y02E60/327 , Y02E60/364 , Y02E60/50
摘要： A hydrogen generator and a fuel cell system including a fuel cell battery and the hydrogen generator. The hydrogen generator includes a cartridge, a housing with a cavity to removably contain the cartridge, and an initiation system. The cartridge includes a casing; a plurality of pellets including a hydrogen containing material; a plurality of solid heat transfer members in contact with but not penetrating the casing; a hydrogen outlet in the casing; and a hydrogen flow path from each pellet to the hydrogen outlet. A plurality of heating elements is disposed inside the housing. When the cartridge is in the cavity, each heating element is disposed so heat can be conducted from the heating element and through the casing and corresponding heat transfer member to initiate the release of hydrogen gas. The initiation system can selectively heat one or more pellets to release hydrogen gas as needed.
摘要翻译： 一种氢发生器和包括燃料电池和氢发生器的燃料电池系统。 氢气发生器包括筒，具有可移除地容纳盒的空腔的壳体和起始系统。 盒包括壳体; 包含含氢材料的多个粒料; 多个固体传热构件，其与壳体接触但不穿透壳体; 壳体中的氢出口; 以及从每个颗粒到氢气出口的氢气流动路径。 多个加热元件设置在壳体内。 当盒位于空腔中时，每个加热元件被设置成使得热量可以从加热元件通过壳体和相应的传热构件传导以开始释放氢气。 起始系统可以根据需要选择性地加热一个或多个粒料以释放氢气。
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公开(公告)号：US20140295304A1
公开(公告)日：2014-10-02
申请号：US14301960
申请日：2014-06-11
发明人： Richard A. Langan , Jason L. Stimits , Chad E. Law , Russell H. Barton , Thomas J. Kmetich , Allison M. Fisher , Guanghong Zheng , Olen Vanderleeden
CPC分类号： H01M8/0643 , C01B3/0005 , C01B3/0084 , C01B3/02 , C01B3/04 , C01B3/08 , C01B2203/085 , C01B2203/1619 , C01B2203/1623 , F17C11/005 , H01M8/04208 , H01M8/04216 , H01M8/0618 , H01M8/065 , Y02E60/321 , Y02E60/324 , Y02E60/327 , Y02E60/364 , Y02E60/50
摘要： A hydrogen generator and a fuel cell system including a fuel cell battery and the hydrogen generator. The hydrogen generator includes a cartridge, a housing with a cavity to removably contain the cartridge, and an initiation system. The cartridge includes a casing; a plurality of pellets including a hydrogen containing material; a plurality of solid heat transfer members in contact with but not penetrating the casing; a hydrogen outlet in the casing; and a hydrogen flow path from each pellet to the hydrogen outlet. A plurality of heating elements is disposed inside the housing. When the cartridge is in the cavity, each heating element is disposed so heat can be conducted from the heating element and through the casing and corresponding heat transfer member to initiate the release of hydrogen gas. The initiation system can selectively heat one or more pellets to release hydrogen gas as needed.
摘要翻译： 一种氢发生器和包括燃料电池和氢发生器的燃料电池系统。 氢气发生器包括筒，具有可移除地容纳盒的空腔的壳体和起始系统。 盒包括壳体; 包含含氢材料的多个粒料; 多个固体传热构件，其与壳体接触但不穿透壳体; 壳体中的氢出口; 以及从每个颗粒到氢气出口的氢气流动路径。 多个加热元件设置在壳体内。 当盒位于空腔中时，每个加热元件被设置成使得热量可以从加热元件通过壳体和相应的传热构件传导以开始释放氢气。 起始系统可以根据需要选择性地加热一个或多个粒料以释放氢气。
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公开(公告)号：US20160104907A1
公开(公告)日：2016-04-14
申请号：US14975485
申请日：2015-12-18
发明人： Richard A. Langan , Jason L. Stimits , Chad E. Law , Russell H. Barton , Thomas J. Kmetich , Allison M. Fisher , Guanghong Zheng , Olen Vanderleeden
CPC分类号： H01M8/0643 , C01B3/0005 , C01B3/0084 , C01B3/02 , C01B3/04 , C01B3/08 , C01B2203/085 , C01B2203/1619 , C01B2203/1623 , F17C11/005 , H01M8/04208 , H01M8/04216 , H01M8/0618 , H01M8/065 , Y02E60/321 , Y02E60/324 , Y02E60/327 , Y02E60/364 , Y02E60/50
摘要： A hydrogen generator and a fuel cell system including a fuel cell battery and the hydrogen generator. The hydrogen generator includes a cartridge, a housing with a cavity to removably contain the cartridge, and an initiation system. The cartridge includes a casing; a plurality of pellets including a hydrogen containing material; a plurality of solid heat transfer members in contact with but not penetrating the casing; a hydrogen outlet in the casing; and a hydrogen flow path from each pellet to the hydrogen outlet. A plurality of heating elements is disposed inside the housing. When the cartridge is in the cavity, each heating element is disposed so heat can be conducted from the heating element and through the casing and corresponding heat transfer member to initiate the release of hydrogen gas. The initiation system can selectively heat one or more pellets to release hydrogen gas as needed.
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公开(公告)号：US20150203353A1
公开(公告)日：2015-07-23
申请号：US14676393
申请日：2015-04-01
发明人： Allison M. Fisher , Guanghong Zheng , Jason L. Stimits , Chad E. Law , Russell H. Barton , Richard A. Langan , Thomas J. Kmetich , Gerald A. Zsigo
CPC分类号： C01B3/001 , B01J19/24 , B01J2219/00076 , B01J2219/24 , C01B3/04 , Y02E60/364
摘要： Disclosed is a fuel unit for a gas generator such as a hydrogen gas generator that can supply gas to a gas consuming system such as a fuel cell system. The fuel unit includes a housing containing a solid fuel composition and a heat producing material. The fuel composition contains gas releasing solid material that reacts to release gas when heated. The heat producing material reacts exothermically to produce heat. A plurality of quantities of the heat producing material are in thermal communication with corresponding portions of an unsegregated quantity the fuel composition such that, following initiation of a reaction of each quantity of the heat producing material, the quantity of heat producing material will heat the corresponding portion of the unsegregated quantity of the fuel composition, and the corresponding portion of the unsegregated quantity of the fuel composition will react to release a quantity of the gas.
摘要翻译： 公开了一种用于诸如氢气发生器的气体发生器的燃料单元，其可以向诸如燃料电池系统的燃气消耗系统供应气体。 燃料单元包括含有固体燃料组合物和发热材料的壳体。 燃料组合物含有释放气体的固体材料，其在加热时反应释放气体。 发热材料放热反应产生热量。 多个量的发热材料与燃料组合物的未分离量的对应部分热连通，使得在每一量的发热材料的反应开始之后，发热材料的量将加热相应的 未分离量的燃料组合物的一部分和燃料组合物的未分离量的相应部分将反应以释放一定量的气体。
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公开(公告)号：US09947947B2
公开(公告)日：2018-04-17
申请号：US14629317
申请日：2015-02-23
IPC分类号： C01B3/00 , H01M8/04082 , C01B35/00 , C01B6/23
CPC分类号： H01M8/04216 , C01B6/23 , C01B35/00
摘要： The invention relates to mixed metal borohydrides used for solid hydrogen storage. The mixed metal borohydrides are synthesized through solution synthesis using multiple metal borohydrides. First and second precursor solutions are prepared and combined to create a mixture in which the mixed metal borohydride is formed. The solvent is removed, leaving the mixed metal borohydride. The first precursor solution consisting essentially of lithium borohydride, and the second precursor solution consisting essentially of a borohydride compound containing one or more metal cations selected from the group of metals consisting of sodium, magnesium, calcium and titanium.
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