Invention Grant
- Patent Title: Purifying crude furan 2,5-dicarboxylic acid by hydrogenation and a purge zone
-
Application No.: US15200467Application Date: 2016-07-01
-
Publication No.: US09944615B2Publication Date: 2018-04-17
- Inventor: Mesfin Ejerssa Janka , Kenny Randolph Parker , Ashfaq Shahanawaz Shaikh , Lee Reynolds Partin , Charles Edwan Sumner, Jr. , Shane Kipley Kirk
- Applicant: EASTMAN CHEMICAL COMPANY
- Applicant Address: US TN Kingsport
- Assignee: EASTMAN CHEMICAL COMPANY
- Current Assignee: EASTMAN CHEMICAL COMPANY
- Current Assignee Address: US TN Kingsport
- Agent Steven A. Owen
- Main IPC: C07D307/68
- IPC: C07D307/68 ; B01D11/04

Abstract:
A process for purifying a crude furan 2,5-dicarboxylic acid composition (cFDCA) by hydrogenation of a FDCA composition dissolved in a hydrogenation solvent such as water, and hydrogenating under mild conditions, such as at a temperature within a range of 130° C. to 225° C. by contacting the solvated FDCA composition with hydrogen in the presence of a hydrogenation catalyst under a hydrogen partial pressure within a range of 10 psi to 900 psi. A product FDCA composition is produced having a low amount of tetrahydrofuran dicarboxylic acid, a low b*, and a low amount of 5-formyl furan-2-carboxylic acid (FFCA).
Public/Granted literature
- US20160311790A1 PURIFYING CRUDE FURAN 2,5-DICARBOXYLIC ACID BY HYDROGENATION AND A PURGE ZONE Public/Granted day:2016-10-27
Information query