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    Methods for deposition of group 4 metal containing films
    1.
    发明公开
    Methods for deposition of group 4 metal containing films 审中-公开
    对于含金属膜4族金属前体

    公开(公告)号：EP2322690A3

    公开(公告)日：2011-06-15

    申请号：EP10188627.3

    申请日：2010-10-22

    申请人： AIR PRODUCTS AND CHEMICALS, INC.

    发明人： Ivanov, Sergei Vladimirovich ,  Lei, Xinjian ,  Cheng, Hansong ,  Spence, Daniel P. ,  Kim, Moo-Sung

    IPC分类号： C23C16/18 ,  C23C30/00 ,  C07F7/00

    CPC分类号： C23C16/45553 ,  C07F7/006 ,  C23C16/405

    摘要： Metal-containing films may be formed by atomic layer deposition using precursors of the formula:

            M(OR 1 )(OR 2 )(R 3 C(O)C(R 4 )C(O)XR 5 y ) 2

    wherein M is Group 4 metals; wherein R 1 and R 2 are independently selected from the group consisting of linear or branched C 1-10 alkyls and C 6-12 aryls; R 3 is selected from the group consisting of linear or branched C 1-10 alkyls and C 6-12 aryls, and is preferably C 1-3 alkyl; R 4 is selected from the group consisting of hydrogen, C 1-10 alkyls, and C 6-12 aryls, and is preferably hydrogen; R 5 is selected from the group consisting of linear or branched C 1-10 alkyls and C 6-12 aryls, and is preferably a methyl or ethyl group; and X = O or N, wherein when X = O, y = 1 and R 1 , 2 and 5 are the same, and when X = N, y = 2 and each R 5 can be the same or different.

    Methods for deposition of group 4 metal containing films
    2.
    发明公开
    Methods for deposition of group 4 metal containing films 审中-公开
    Gruppe-4-Metallvorläuferfürmetallhaltige Filme

    公开(公告)号：EP2322690A2

    公开(公告)日：2011-05-18

    申请号：EP10188627.3

    申请日：2010-10-22

    申请人： AIR PRODUCTS AND CHEMICALS, INC.

    发明人： Ivanov, Sergei Vladimirovich ,  Lei, Xinjian ,  Cheng, Hansong ,  Spence, Daniel P. ,  Kim, Moo-Sung

    IPC分类号： C23C16/18 ,  C23C30/00 ,  C07F7/00

    CPC分类号： C23C16/45553 ,  C07F7/006 ,  C23C16/405

    摘要： Metal-containing films may be formed by atomic layer deposition using precursors of the formula:

    wherein M is Group 4 metals; wherein R 1 and R 2 are independently selected from the group consisting of linear or branched C 1-10 alkyls and C 6-12 aryls; R 3 is selected from the group consisting of linear or branched C 1-10 alkyls and C 6-12 aryls, and is preferably C 1-3 alkyl; R 4 is selected from the group consisting of hydrogen, C 1-10 alkyls, and C 6-12 aryls, and is preferably hydrogen; R 5 is selected from the group consisting of linear or branched C 1-10 alkyls and C 6-12 aryls, and is preferably a methyl or ethyl group; and X = O or N, wherein when X = O, y = 1 and R 1 , 2 and 5 are the same, and when X = N, y = 2 and each R 5 can be the same or different.

    摘要翻译： 含金属膜可以通过原子层沉积形成，使用下式的前体：€ƒ€ƒ€ƒ€ƒ€ƒM（OR 1）（OR 2）（R 3 C（O）C R 4）C（O）XR 5 y）2其中M是4族金属; 其中R 1和R 2独立地选自直链或支链C 1-10烷基和C 6-12芳基; R 3选自直链或支链C 1-10烷基和C 6-12芳基，优选C 1-3烷基; R 4选自氢，C 1-10烷基和C 6-12芳基，优选为氢; R 5选自直链或支链C 1-10烷基和C 6-12芳基，优选甲基或乙基; 并且X = O或N，其中当X = O时，y = 1且R 1,2和5相同，并且当X = N，y = 2且每个R 5可以相同或不同时。

    Group 4 metal precursors for metal-containing films
    6.
    发明公开
    Group 4 metal precursors for metal-containing films 有权
    第4族金属前体用于含金属膜

    公开(公告)号：EP2322530A2

    公开(公告)日：2011-05-18

    申请号：EP10188585.3

    申请日：2010-10-22

    申请人： AIR PRODUCTS AND CHEMICALS, INC.

    发明人： Ivanov, Sergei Vladimirovich ,  Lei, Xinjian ,  Cheng, Hansong ,  Spence, Daniel P. ,  Kim Moo-Sung

    IPC分类号： C07F7/00 ,  C23C30/00 ,  C23C16/18

    CPC分类号： C23C16/18 ,  C07F7/006 ,  C23C16/405 ,  C23C16/45553 ,  Y02P20/582

    摘要： Group 4 metal containing films may be deposited using a new family of Group 4 metal precursors represented by the formula:

    wherein M is a Group 4 metals of Ti, Zr, or Hf; wherein R 1 is selected from the group consisting of linear or branched C 1-10 alkyls and C 6-12 aryls, and is preferably methyl, ethyl or n-propyl; R 2 is selected from the group consisting of branched C 3-10 alkyls and C 6-12 aryls, and is preferably iso-propyl, tert-butyl, sec-butyl, iso-butyl, or tert-amyl; and R 3 is selected from the group consisting of hydrogen, C 1-10 alkyls, and C 6-12 aryls, and is preferably hydrogen. In a preferred embodiment of this invention, the precursor is a liquid or a solid with a melting point below 60°C.

    摘要翻译： 可使用由下式表示的第4族金属前体族来沉积含第4族金属的膜：其中M为Ti，Zr或Hf的第4族金属; 其中R 1选自直链或支链C 1-10烷基和C 6-12芳基，并且优选为甲基，乙基或正丙基; R2选自由支链C 3-10烷基和C 6-12芳基组成的组，并且优选为异丙基，叔丁基，仲丁基，异丁基或叔戊基; 并且R3选自氢，C1-10烷基和C6-12芳基，并且优选为氢。 在本发明的一个优选实施方案中，前体是熔点低于60℃的液体或固体。

    Stable electrolyte counteranions for electrochemical devices
    7.
    发明公开
    Stable electrolyte counteranions for electrochemical devices 审中-公开
    Stabile Elektrolyt-Gegenanionenfürelektrochemische Vorrichtungen

    公开(公告)号：EP1763099A2

    公开(公告)日：2007-03-14

    申请号：EP06017458.8

    申请日：2006-08-22

    申请人： AIR PRODUCTS AND CHEMICALS, INC.

    发明人： Pez, Guido Peter ,  Ivanov, Sergei Vladimirovich ,  Dantsin, Gennady ,  Casteel, William Jack ,  Lehmann, John F.

    IPC分类号： H01M6/16 ,  H01M10/40 ,  H01B1/12

    CPC分类号： H01M10/0567 ,  H01B1/122 ,  H01M6/166 ,  H01M10/052 ,  H01M10/0568 ,  H01M2300/0017 ,  Y02T10/7011

    摘要： The invention relates to electrolyte salts for electrochemical devices of improved physical, chemical and electrochemical stability.
    The improvement resides in the use of anions of salts of the formula comprising:
    i) (B 12 F x Z 12-x ) 2- wherein Z comprises at least one of H, Cl, Br or OR; R comprises at least one of H, alkyl or fluoroalkyl, or at least one polymer and x is at least 3 on an average basis but not more than 12;
    ii) ((R'R''R''')NB 12 F x Z (11-x) ) - , wherein N is bonded to B and each of R', R", R''' comprise a member independently selected from the group consisting of hydrogen, alkyl, cycloalkyl, aryl and a polymer; Z comprises H, Cl, Br, or OR, where R comprises H, alkyl or perfluoroalkyl or a polymer, and x is an integer from 0 to 11; or
    iii) (R""CB 11 F x Z (11-x) ) - , wherein R"" is bonded to C and comprises a member selected from the group consisting of hydrogen, alkyl, cycloalkyl, aryl, and a polymer, Z comprises H, Cl, Br, or OR, wherein R comprises H, alkyl or perfluoroalkyl or a polymer, and x is an integer from 0 to 11.

    摘要翻译： 本发明涉及具有改进的物理，化学和电化学稳定性的电化学装置的电解质盐。 改进在于使用下式的盐阴离子，包括：i）（B 12 F x Z 12-x）2-其中Z包括H，Cl，Br或OR中的至少一个; R包括H，烷基或氟烷基或至少一种聚合物中的至少一种，x平均为至少3，但不超过12; ii）（（R'R''R“'）NB 12 F x Z（11-x）） - ，其中N键合到B，R'，R”，R“'各自独立地包括一个成员 选自氢，烷基，环烷基，芳基和聚合物; Z包括H，Cl，Br或OR，其中R包括H，烷基或全氟烷基或聚合物，x是0至11的整数; 或iii）（R“”CB 11 F x Z（11-x）） - ，其中R“”与C键合，并且包含选自氢，烷基，环烷基，芳基和聚合物的成员， Z包括H，Cl，Br或OR，其中R包括H，烷基或全氟烷基或聚合物，x是0至11的整数。

    Process for producing boranes
    8.
    发明公开
    Process for producing boranes 有权
    Verfahren zur Herstellung von Boranen

    公开(公告)号：EP1734004A1

    公开(公告)日：2006-12-20

    申请号：EP06012257.9

    申请日：2006-06-14

    申请人： Air Products and Chemicals, Inc.

    发明人： Ivanov, Sergei Vladimirovich ,  Casas, Baldomero

    IPC分类号： C01B35/02

    CPC分类号： C01B35/026 ,  C07F5/022

    摘要： This idea relates to the synthesis of salts of dodecahydrododecaborate B12H12 (2-). In the proposed process a metal hydride is reacted with an alkyl borate in the presence of a Lewis base to produce Lewis base-borane complex, which is thermally decomposed to produce salts of B12H12 (2-), while alkyl borate is recovered from the reaction by-product and is recycled.

    摘要翻译： 这个想法涉及十二氢十二硼酸盐B12H12（2-）的盐的合成。 在所提出的方法中，金属氢化物与路易斯碱存在下的硼酸烷基酯反应以产生路易斯碱 - 硼烷络合物，其被热分解以产生B12H12（2-）的盐，而从反应中回收烷基硼酸盐 副产品并被回收利用。

    Novel copper complexes for CO and olefin adsorption
    9.
    发明公开
    Novel copper complexes for CO and olefin adsorption 审中-公开
    新的铜配合物对CO和烯烃的吸附

    公开(公告)号：EP1048344A2

    公开(公告)日：2000-11-02

    申请号：EP00109003.4

    申请日：2000-04-26

    申请人： AIR PRODUCTS AND CHEMICALS, INC.

    发明人： Strauss, Steven Howard ,  Polyakov, Oleg Gennadievich ,  Hammel, John Wesley ,  Ivanov, Svetlana Mechaelovna ,  Ivanov, Sergei Vladimirovich

    IPC分类号： B01J20/02 ,  B01J20/18 ,  B01D53/02 ,  B01D53/62

    CPC分类号： B01J20/22 ,  B01D53/02

    摘要： A solid state composition is provided having the formula Cu(A) n Z, where A is CO or olefin, n > 1 and Z is a unitary or composite monovalent anion. Further provided are an apparatus adapted to adsorb and a method for adsorbing an adsorbate A from a fluid mixture. The apparatus and method employ an adsorbent having the formula Cu(A) n Z, where A is CO or olefin, n ≥ 0 and Z is a unitary or composite monovalent anion. Z can be selected from the group consisting of: a) X - where X - is BF 4 - , PF 6 - or SbF 6 - ; b) (Al x (OR) y ) - where R is fluoroalkyl or perfluoroalkyl, and x is 0 and y is 1, or x is 1 and y is 4; c) (RCO 2 ) - where R is alkyl, fluoroalkyl, perfluoroalkyl, aryl, fluoroaryl or perfluoroaryl; d) (RSO 3 ) - where R is alkyl, fluoroalkyl, perfluoroalkyl, aryl, fluoroaryl or perfluoroaryl; e) (H(RCO 2 ) 2 ) - where R is alkyl, fluoroalkyl, perfluoroalkyl, aryl, fluoroaryl or perfluoroaryl; f) (H(RSO 3 ) 2 ) - where R is alkyl, fluoroalkyl, perfluoroalkyl, aryl, fluoroaryl or perfluoroaryl; g) (N(SO 2 R) x R' y ) - where R is fluoroalkyl, perfluoroalkyl, aryl, fluoroaryl or perfluoroaryl, R' is alkyl, fluoroalkyl, perfluoroalkyl, aryl, fluoroaryl or perfluoroaryl, x + y = 2 and x = 1 or 2; h) (C(SO 2 R) x R' y ) - where R is fluoroalkyl, perfluoroalkyl, aryl, fluoroaryl or perfluoroaryl, R' is hydrogen, alkyl, fluoroalkyl, perfluoroalkyl, aryl, fluoroaryl or perfluoroaryl, x + y = 3 and x = 1, 2 or 3; i) (CB 11 H 12-m X m ) - where m is from 0 to 12, and X is at least one member selected from the group consisting of halogen, alkyl, fluoroalkyl, perfluoroalkyl, aryl, fluoroaryl and perfluoroaryl; j) (CB 9 H 10-m X m ) - where m is from 0 to 10, and X is at least one member selected from the group consisting of halogen, alkyl, fluoroalkyl, perfluoroalkyl, aryl, fluoroaryl and perfluoroaryl; and k) (CB 11 F 11 R) - where R is alkyl, fluoroalkyl, perfluoroalkyl, aryl, fluoroaryl, perfluoroaryl or ammonium.