PROCESS FOR THE PRODUCTION OF MONOLITHS BY MEANS OF THE SOL-GEL PROCESS
    2.
    发明公开
    PROCESS FOR THE PRODUCTION OF MONOLITHS BY MEANS OF THE SOL-GEL PROCESS 审中-公开
    通过溶胶 - 凝胶法生产单晶体的方法

    公开(公告)号:EP1858815A1

    公开(公告)日:2007-11-28

    申请号:EP06708245.3

    申请日:2006-02-14

    摘要: Process for the production of monoliths of glass by means of the sol-gel process, comprising the following steps: a) dispersion in water of an oxide prepared by the pyrogenic route, b) hydrolysis of an alkoxide in aqueous solution to form a hydrolysate, c) mixing of the hydrolysate of the alkoxide with the oxide prepared by the pyrogenic route to form a colloidal sol, d) optional removal of coarse contents from the colloidal sol, e) gelling of the colloidal sol in a mould, f) replacement of the water contained in the resulting aerogel by an organic solvent, g) drying of the aerogel, h) heat treatment of the dried aerogel.

    摘要翻译: 该方法包括以下步骤:a)通过热解途径制备的氧化物在水中的分散,b)醇盐在水溶液中的水解以形成水解产物, c)将醇盐的水解产物与通过热解途径制备的氧化物混合以形成胶体溶胶,d)任选地从胶体溶胶中除去粗颗粒,e)胶体溶胶在模具中胶凝,f) 所得到的气凝胶中含有的有机溶剂中的水,g)气凝胶的干燥,h)干燥后的气凝胶的热处理。