A SHAPE CONTROLLED PRO-CATALYST AND A SINGLE POT PROCESS FOR PREPARING THE SAME
    103.
    发明公开
    A SHAPE CONTROLLED PRO-CATALYST AND A SINGLE POT PROCESS FOR PREPARING THE SAME 审中-公开
    德国皇家赫尔辛顿大学的制造商PRO-KATALYSATOR

    公开(公告)号:EP3157893A2

    公开(公告)日:2017-04-26

    申请号:EP15796664.9

    申请日:2015-05-22

    摘要: The present disclosure relates to a single-pot multi step process for the preparation of a shape controlled pro-catalyst. The process comprises the steps of: i. reacting magnesium metal and at least one alkanol to obtain spheroidal magnesium alkoxide; ii. treating the spheroidal magnesium alkoxide with at least one transition metal tetrahalide, at least one organic modifier, and optionally, at least one in-organic modifier in the presence of at least one solvent to obtain a reaction mixture; iii. cooling, settling the reaction mixture and decanting the supernatant; iv. adding at least one transition metal tetrahalide, at least one solvent and optionally, at least one organic or inorganic modifier; and v. iterating steps (iii) and (iv) to obtain the shape controlled pro-catalyst.

    摘要翻译: 本公开内容涉及用于制备形状控制的前催化剂的单罐多步骤方法。 该过程包括以下步骤:i。 使镁金属与至少一种链烷醇反应得到球形醇镁; II。 在至少一种溶剂的存在下用至少一种过渡金属四卤化物,至少一种有机改性剂和任选的至少一种有机内改性剂处理球形镁醇盐以获得反应混合物; III。 冷却,沉降反应混合物并倾析上清液; IV。 加入至少一种过渡金属四卤化物,至少一种溶剂和任选的至少一种有机或无机改性剂; 和v。重复步骤(iii)和(iv)以获得形状控制的促催化剂。

    METHOD FOR PRODUCING MAGNESIUM ALCOHOLATE
    105.
    发明公开
    METHOD FOR PRODUCING MAGNESIUM ALCOHOLATE 有权
    方法ZUR HERSTELLUNG VON MAGNESIUMALKOHOLAT

    公开(公告)号:EP2754648A4

    公开(公告)日:2015-05-13

    申请号:EP12841454

    申请日:2012-10-12

    申请人: NIPPON SODA CO

    发明人: KOBAYASHI HITOSHI

    IPC分类号: C07C29/70 C07C31/30 C08F4/06

    摘要: The purpose of the present invention is to provide a spherical or ellipsoidal magnesium alcoholate having a narrow particle size distribution even when the particle size is small. The present invention provides a method for producing a magnesium alcoholate by adding in a portionwise manner to a reaction system and reacting, metallic magnesium, an alcohol, and at least one of a halogen or a halogen atom-containing compound in the reaction system under alcohol reflux, which is a method for producing a magnesium alcoholate characterized in that a mixture of metallic magnesium, an alcohol, and at least one of a halogen or a halogen atom-containing compound is added to the reaction system at each portionwise addition.

    摘要翻译: 本发明的目的是提供即使在粒径小的情况下也具有窄的粒度分布的球形或椭圆形醇镁化物。 本发明提供了一种通过向反应体系中分批加入并在醇的反应体系中使金属镁,醇和至少一种含卤素或含卤原子的化合物反应来制备醇镁的方法 回流,其是产生镁醇盐的方法,其特征在于每次分批加入将金属镁,醇和至少一种卤素或含卤原子的化合物的混合物加入到反应体系中。

    VERFAHREN ZUR DESTILLATIVEN AUFARBEITUNG EINES METHANOL/WASSER-GEMISCHS SOWIE VERFAHREN ZUR HERSTELLUNG VON ALKALIMETHYLATEN
    107.
    发明公开
    VERFAHREN ZUR DESTILLATIVEN AUFARBEITUNG EINES METHANOL/WASSER-GEMISCHS SOWIE VERFAHREN ZUR HERSTELLUNG VON ALKALIMETHYLATEN 审中-公开
    法进行处理的蒸馏甲醇/水混合物及其制造方法的碱金属甲醇

    公开(公告)号:EP2401045A1

    公开(公告)日:2012-01-04

    申请号:EP10703905.9

    申请日:2010-02-17

    申请人: BASF SE

    摘要: The invention relates to a method for the distillative processing of a methanol/water mixture, wherein a methanol/water mixture is added to a distillation column (1), a vapor stream substantially comprising methanol is removed at the head of the distillation column (1), and a bottom stream substantially comprising water is withdrawn at the base of the distillation column (1), at least part of the vapor stream substantially comprising methanol is condensed and the condensed vapor stream is added as heating vapor to an evaporator (11), in which at least part of the methanol/water mixture to be separated is vaporized. The invention further relates to a method for producing alkali methylates in a reaction column (31), wherein methanol and alkaline lye are added to the reaction column (31). At the lower end of the reaction column (31), alkali methylate dissolved in methanol is withdrawn, and a methanol/water mixture is withdrawn at the upper end of the reaction column (31) and the methanol/water mixture is processed by way of the method for distillative processing.