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    PROCESS FOR THE PREPARATION OF CONDENSED PHOSPHORIC ESTERS
    22.
    发明公开
    PROCESS FOR THE PREPARATION OF CONDENSED PHOSPHORIC ESTERS 有权
    VERFAHREN ZUR HERSTELLUNG KONDENSIERTERPHOSPHORSÄÈLE​​STER

    公开(公告)号：EP1191029A4

    公开(公告)日：2004-03-24

    申请号：EP99954438

    申请日：1999-11-08

    申请人： DAIHACHI CHEM IND

    发明人： NAKAMURA SHIN ,  NOGUCHI KAZUO ,  FUJISAWA TAKU ,  OHKAWA TAKAFUMI

    IPC分类号： C07F9/12 ,  C07F9/14 ,  C09K21/12

    CPC分类号： C09K21/12 ,  C07F9/12 ,  C07F9/1406

    摘要： A process for the preparation of condensed phosphoric esters extremely lowered in volatiles content, which comprises the first step of reacting a phosphorus oxytrihalide with a bisphenol to prepare a phosphorohalidate, the second step of removing unreacted phosphorus oxytrihalide, and the third step of reacting the phosphorohalidate with a monophenol at a specific ratio.

    摘要翻译： 一种制备浓缩磷酸酯的方法，其挥发物含量极低，该方法包括使含氧三卤化磷与双酚反应以制备卤代磷酸酯的第一步，除去未反应的含氧三卤化磷的第二步和使卤代磷酸酯 与一种特定比例的单酚混合。

    PROCESS FOR PRODUCING PHOSPHOROHALIDATE
    24.
    发明公开
    PROCESS FOR PRODUCING PHOSPHOROHALIDATE 有权
    生产磷酸酰胺的方法

    公开(公告)号：EP1153929A1

    公开(公告)日：2001-11-14

    申请号：EP00902011.6

    申请日：2000-01-28

    申请人： DAIHACHI CHEMICAL INDUSTRY CO., LTD.

    发明人： FUJITA, Yasunori

    IPC分类号： C07F9/12 ,  C07F9/14

    CPC分类号： C07F9/1406 ,  C07F9/12

    摘要： The present invention provides a process for producing phosphorohalidate characterized in that a crude reaction product obtained by reacting a phosphorus oxyhalide with an aromatic hydroxy compound in the presence of a Lewis acid catalyst is purified by distillation in the presence of an alkali metal salt. The process of the invention produces a high-purity phosphorohalidate in high yield which contains no impurities such as the phosphorus oxihalidate and aromatic hydroxy compound used as starting materials and the catalyst.

    摘要翻译： 本发明提供了一种生产囟代磷酸酯的方法，其特征在于通过在碱金属盐存在下通过蒸馏纯化通过将卤氧化磷与芳族羟基化合物在路易斯酸催化剂存在下反应而获得的粗反应产物。 本发明的方法以高产率生产高纯度的卤代磷酸酯，其不含杂质，例如用作起始材料的磷酰卤和芳族羟基化合物以及催化剂。

    PROCESS FOR PREPARATION OF PHOSPHORIC ESTERS
    29.
    发明公开
    PROCESS FOR PREPARATION OF PHOSPHORIC ESTERS 有权
    VERFAHREN ZUR HERSTELLUNG VONPHOSPHORSÄUREESTERN

    公开(公告)号：EP1403272A4

    公开(公告)日：2004-12-03

    申请号：EP02724648

    申请日：2002-04-25

    申请人： DAIHACHI CHEM IND

    发明人： TAMURA KAZUNARI

    IPC分类号： C07F9/12 ,  C07F9/14

    CPC分类号： C07F9/1406 ,  C07F9/12

    摘要： A process for preparation of phosphoric esters which comprises step (1) of reacting phosphorus oxychloride with naphthol at a molar ratio of not larger than 1/1.3 in the presence of a metal halide and removing unreacted phosphorus oxychloride and step (2) of reacting the reaction product of step (1) with phenol at a molar ratio (of chlorine contained in the reaction product to phenol) ranging from 1 : 1 to 1 : 1.5 and removing hydrogen chloride formed by a by-product to thereby obtain a phosphoric ester represented by the general formula (I): (1) wherein n is 1 or 2.

    摘要翻译： 一种磷酸酯的制造方法，其特征在于，在金属卤化物存在下，使三氯氧化磷与萘酚以1 / 1.3以下的摩尔比反应，除去未反应的三氯氧化磷的工序（1） 将步骤（1）与苯酚的反应产物以1:1至1:1.5的摩尔比（反应产物与苯酚中所含氯的摩尔比）在1:1至1:1.5范围内，并除去副产物形成的氯化氢，从而获得代表的磷酸酯 由通式（I）表示：（1）其中n是1或2。

    PROCESS FOR THE PREPARATION OF CONDENSED PHOSPHORIC ESTERS
    30.
    发明公开
    PROCESS FOR THE PREPARATION OF CONDENSED PHOSPHORIC ESTERS 有权
    PRODUCING缩合磷酸酯的方法

    公开(公告)号：EP1199310A4

    公开(公告)日：2002-10-02

    申请号：EP99954439

    申请日：1999-11-08

    申请人： DAIHACHI CHEM IND

    发明人： NAKAMURA SHIN ,  NOGUCHI KAZUO ,  FUJISAWA TAKU ,  OHKAWA TAKAFUMI

    IPC分类号： C07F9/12 ,  C07F9/14 ,  C08G79/04

    CPC分类号： C07F9/1406 ,  C07F9/12

    摘要： A process comprising the first step of reacting a phosphorus oxytrihalide with a bisphenol A derivative at a specific ratio to prepare a phosphorohalidate, the second step of removing unreacted phosphorus oxytrihalide, the third step of reacting the reaction product obtained in the second step with a monophenol at 120°C or below, and the fourth step of reacting the phosphorohalidate with a monophenol at 120°C or above. The condensed phosphoric esters obtained by this process are extremely lowered in the content of isopropenylphenyl diphenyl phosphate, which is causative of a lowering in the heat resistance of a resin and staining of molds occurring in molding a resin, when the condensed phosphoric ester is used as an additive for the resin.