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    AUTOSAMPLER
    1.
    发明公开
    AUTOSAMPLER 审中-公开

    公开(公告)号：EP3978918A1

    公开(公告)日：2022-04-06

    申请号：EP21199133.6

    申请日：2021-09-27

    申请人： Thermo Fisher Scientific (Bremen) GmbH ,  Thermo Fisher Scientific S.p.A

    发明人： ZILIOLI, Giacinto ,  BRODIE, Christopher ,  GRIEP-RAMING, Jens

    IPC分类号： G01N30/24 ,  G01N35/04 ,  G01N35/10

    摘要： An autosampler 100 for dispensing samples is provided. The autosampler comprises a sample tray 120 for holding the samples to be dispensed. The sample tray 120 is moveable between a plurality of dispensing positions. The autosampler 100 also comprises a noncontact coupling configured to move the sample tray 120 between the plurality of dispensing positions. An autosampler 100 for dispensing samples is also provided, comprising: a sample tray 120 for holding the samples to be dispensed, the sample tray 120 being moveable between a plurality of dispensing positions, the sample tray 120 and a body 110 of the autosampler 100 comprising respective contact surfaces that contact each other as the sample tray 120 moves between the plurality of dispensing positions, wherein the contact surface of at least one of the sample tray 120 and the body 110 of the autosampler 100 comprises a self-lubricating material.

    METHOD AND DEVICE FOR VAPORIZATION INJECTION OF HIGH VOLUMES IN GAS CHROMATOGRAPHIC ANALYSIS
    3.
    发明授权
    METHOD AND DEVICE FOR VAPORIZATION INJECTION OF HIGH VOLUMES IN GAS CHROMATOGRAPHIC ANALYSIS 有权

    公开(公告)号：EP1459060B1

    公开(公告)日：2018-08-22

    申请号：EP02788384.2

    申请日：2002-12-19

    申请人： Thermo Fisher Scientific S.p.A

    发明人： MAGNI, Paolo ,  PORZANO, Thomas

    IPC分类号： G01N30/12 ,  G01N30/16

    CPC分类号： G01N30/16 ,  G01N30/12 ,  G01N2030/025 ,  G01N2030/127 ,  G01N2030/165 ,  G01N2030/167

    摘要： This invention concerns a method and apparatus for vaporization injection of large volumes of liquid sample (substance to be analysed+solvent) introduced by a syringe needle into a heated vaporization chamber which is part of an injector coupled operatively to a device for gas chromatographic analysis. The sample is sent in the form of a liquid band traveling through the vaporization chamber at high speed until it reaches a stopping and vaporization device positioned adjacent to the inlet of a capillary to collect the vapors. In order to inject large volumes without modifying the vaporization chamber and without partial losses of the samples, the sample vapors, in splitless mode, are drawn up from the vaporization chamber into the capillary by virtue of the local action of volume contraction caused by recondensation of at least the solvent vapors in the capillary.

    MODULAR GAS CHROMATOGRAPH
    4.
    发明公开
    MODULAR GAS CHROMATOGRAPH 有权
    模块气体色谱

    公开(公告)号：EP2417447A1

    公开(公告)日：2012-02-15

    申请号：EP09787696.5

    申请日：2009-04-06

    申请人： Thermo Fisher Scientific S.p.A

    发明人： ZILIOLI, Giacinto ,  PELAGATTI, Stefano ,  MAGNI, Paolo

    IPC分类号： G01N30/88

    CPC分类号： G01N30/88 ,  G01N30/24 ,  G01N30/62 ,  G01N2030/025 ,  G01N2030/8881

    摘要： This invention is related to a gas chromatograph wherein more substitutable modules are foreseen, in particular injector modules and/or detector modules, as well as one embodiment in an oven module. Each module is insertable in a seat of the gas chromatograph mainframe with fast connections of its electronic and pneumatic means to corresponding outlets on said mainframe. Each module has its own heating element.

    摘要翻译： 本发明涉及一种气相色谱仪，其中预见了更多可替代的模块，特别是喷射器模块和/或检测器模块，以及炉模块中的一个实施例。 每个模块都可插入气相色谱仪主机座的座内，并将其电子和气动装置快速连接到所述主机上的相应出口。 每个模块都有自己的加热元件。

    APPARATUS HAVING ONE OR MORE SENSORS FOR SAMPLING THE HEADSPACE AND PROCESS FOR SAMPLING THE HEADSPACE
    7.
    发明公开
    APPARATUS HAVING ONE OR MORE SENSORS FOR SAMPLING THE HEADSPACE AND PROCESS FOR SAMPLING THE HEADSPACE 审中-公开

    公开(公告)号：EP3578968A1

    公开(公告)日：2019-12-11

    申请号：EP19178014.7

    申请日：2019-06-04

    申请人： Thermo Fisher Scientific S.p.A

    发明人： BOSAGLIA, Tiziano ,  FACCHETTI, Riccardo ,  PETTENON, Eugenio ,  ANTONIUCCI, Flavio

    IPC分类号： G01N30/12 ,  G01N30/24 ,  G01N1/22 ,  G01N30/16

    摘要： The present invention relates to an apparatus (1) for sampling the headspace, comprising: a mobile station (2) provided with a plurality of housing seats (21) to house a plurality of containers (100) for sampling the headspace; an oven (3); a blocking device (4) comprising at least one first mobile element (41) that moves between a first position adapted to prevent a container (100) from passing from the mobile station (2) to the oven (3), and a second position adapted to allow a container (100) to pass from the mobile station (2) to the oven (3); at least one first sensor (5a) placed upstream of the first mobile element (41), to detect the presence of a container (100) in a housing seat (21); a movement element (6) moving between said mobile station (2) and the oven (3), the movement element being configured to move a container (100) from the mobile station (2) to the oven (3).

    ELEMENTAL ANALYSER
    10.
    发明公开
    ELEMENTAL ANALYSER 审中-公开
    元素分析仪

    公开(公告)号：EP3306312A1

    公开(公告)日：2018-04-11

    申请号：EP16425096.1

    申请日：2016-10-10

    申请人： Thermo Fisher Scientific S.p.A

    发明人： Galotta, Walter ,  Magni, Andrea ,  Krotz, Liliana ,  Leone, Francesco

    IPC分类号： G01N31/12 ,  G01N30/66

    CPC分类号： G01N30/66 ,  G01N30/02 ,  G01N30/20 ,  G01N31/12 ,  G01N2030/025 ,  G01N2030/8405

    摘要： The invention relates to elemental analysers and, in particular, but not exclusively, organic elemental analysers and isotope ratio mass spectrometry (IRMS) elemental analysers.
    An analysis system for analysing the constituents of a sample of material, the system comprising: a reference supply conduit (2) for supplying a source of a first gas (70a); a carrier supply conduit (4) for supplying a source of the first (70a) or a second gas (70b); first (30a) and second (30b) reactors; a first auto-sampler (20a) for providing one or more samples of material, the first auto-sampler (20a) having an inlet (22a) for receiving gas and an outlet (23a) for providing the received gas and a sample to the first reactor (30a); a second auto-sampler (20b) for providing one or more samples of material, the second auto-sampler (20b) having an inlet (22b) for receiving gas and an outlet (23b) for providing the received gas and a sample to the second reactor (30b); a thermal conductivity detector (10) having first (15) and second channels (13) for identifying the relative conductivity of the gases in each channel, characterised in that: the system further comprises a valve system (80, 100) arranged to control the flow of gas from the supply conduits (2,4) to the inlets (22a, 22b) of the first (20a) and second (20b) auto-samplers; the analysis system has a first mode of operation in which:
    • the valve system (80, 100) connects the carrier supply conduit (4) with the first auto-sampler (20a);
    • the first auto-sampler (20a) delivers the received gas and a sample to the first reactor (30a);
    • the first reactor (30a) delivers at least one reaction product to one channel of the thermal conductivity detector; and
    • the valve system (80, 100) connects the reference supply conduit (2) to the other channel of the thermal conductivity detector (10); and
    the analysis system has a second mode of operation in which:
    • the valve system (105) connects the carrier supply conduit (4) with the second auto-sampler (20b);
    • the second auto-sampter (20b) delivers the received gas and a sample to the second reactor (30b);
    • the second reactor (30b) delivers at least one reaction product to one channel of the thermal conductivity detector (10); and
    • the valve system (80, 100) connects the reference supply conduit (2) to the other channel of the thermal conductivity detector (10).

    摘要翻译： 本发明涉及元素分析仪，尤其涉及但不限于有机元素分析仪和同位素比质谱（IRMS）元素分析仪。 一种用于分析材料样品成分的分析系统，该系统包括：用于供应第一气体源（70a）的参考供应管道（2） 用于供应第一气体（70a）或第二气体（70b）的源的载体供应导管（4）; 第一（30a）和第二（30b）反应器; （20a），其用于提供一个或多个材料样本，所述第一自动采样器（20a）具有用于接收气体的入口（22a）和用于向所述第一自动采样器（20a）提供所接收的气体和样本的出口（23a） 第一反应器（30a）; 用于提供一个或多个材料样本的第二自动采样器（20b），所述第二自动采样器（20b）具有用于接收气体的入口（22b）和用于将所接收的气体和样本提供给 第二反应器（30b）; 具有用于识别每个通道中的气体的相对电导率的第一通道（15）和第二通道（13）的热导率检测器（10），其特征在于：所述系统还包括阀系统（80,100），所述阀系统 气体从第一（20a）和第二（20a）和第二（20b）自动采样器的供应导管（2,4）流入入口（22a，22b） 分析系统具有第一操作模式，其中：·阀系统（80,100）将载体供应导管（4）与第一自动采样器（20a）连接; ·第一自动采样器（20a）将所接收的气体和样品输送到第一反应器（30a）; ·第一反应器（30a）将至少一种反应产物输送到热导检测器的一个通道; 以及·阀系统（80,100）将参考供应导管（2）连接到热导检测器（10）的另一通道; 并且分析系统具有第二操作模式，其中：·阀系统（105）将载体供应导管（4）与第二自动采样器（20b）连接; ·第二自动采样器（20b）将所接收的气体和样本输送到第二反应器（30b）; ·第二反应器（30b）将至少一种反应产物输送到热导检测器（10）的一个通道; 和·阀门系统（80,100）将参考供应管道（2）连接到热导检测器（10）的另一个通道。