Methods of producing n-alkoxycarbonylpiperidine derivatives and intermediates therefor
    2.
    发明公开
    Methods of producing n-alkoxycarbonylpiperidine derivatives and intermediates therefor 有权
    一种用于N-烷氧羰基 - 哌啶衍生物的制备,以及其中间体的过程

    公开(公告)号:EP1400511A1

    公开(公告)日:2004-03-24

    申请号:EP03020567.8

    申请日:2003-09-17

    IPC分类号: C07D211/46

    CPC分类号: C07D211/46

    摘要: A method of producing an N-alkoxycarbonylpiperidine derivative, comprising reacting an N-aralkylpiperidine derivative represented by the following general formula (1):
    with a mesyl halide in the presence of a base, thereby obtaining a mesylated product and reacting the mesylated product with a dicarbonate represented by the following general formula (3):
    wherein R 4 represents an alkyl group, in the presence of hydrogen and a catalyst containing palladium, thereby obtaining an N-alkoxycarbonylpiperidine derivative represented by the following general formula (4):
    wherein R 4 represents an alkyl group and Ms represents a mesyl group.

    摘要翻译: 生产N- alkoxycarbonylpiperidine衍生物的方法,包括使由以下通式表示的N- aralkylpiperidine衍生物(1):在碱的存在下,甲磺酰卤化物,从而获得甲磺酰化产物和使下甲磺酰化 产物与下述通式(3)表示的二碳酸酯: worinř<4> darstellt烷基,在氢和催化剂存在下含有钯,由此获得由以下通式代表的N- alkoxycarbonylpiperidine衍生物 式(4): worinř<4> darstellt烷基及Ms darstellt甲磺酰基。

    Poly 1,2,2-Trimethyl-1-phenyl disilane and method for producing the same
    8.
    发明公开
    Poly 1,2,2-Trimethyl-1-phenyl disilane and method for producing the same 失效
    聚1,2,2-三甲基-1-苯基二氯硅烷和Verfahren zur Herstellung。

    公开(公告)号:EP0252391A2

    公开(公告)日:1988-01-13

    申请号:EP87109258.1

    申请日:1987-06-27

    IPC分类号: C08G77/60

    CPC分类号: C08G77/60

    摘要: A 1,2,2-trimethyl-1-phenylpolydisilane is prepared by condensating 1,2-dichloro-1,2,2-trimethyl-1-phenyl- disilane in the presence of an alkali metal or alkali earth metal, in an aprotic solvent. This polymer is a viscous liquid which has a weight average molecular weight in the range of from 5,000 to 500,000 and a narrow molecular weight distribution, and has various uses as electroconductors, photoresist and optical information recording materials.

    摘要翻译: 在碱金属或碱土金属的存在下,在非质子传递溶剂中使1,2-二氯-1,2,2-三甲基-1-苯基二硅烷缩合制备1,2,2-三甲基-1-苯基聚硅烷。 该聚合物是重均分子量在5000至500,000范围内并具有窄分子量分布的粘性液体,并且具有各种用途作为电导体,光致抗蚀剂和光学信息记录材料。

    NON-DELIQUESCENT ACID ADDITION SALT OF 3-AMINOQUINUCLIDINE
    9.
    发明公开
    NON-DELIQUESCENT ACID ADDITION SALT OF 3-AMINOQUINUCLIDINE 审中-公开
    3-氨基喹啉不加去酸添加盐

    公开(公告)号:EP3279199A1

    公开(公告)日:2018-02-07

    申请号:EP16773148.8

    申请日:2016-03-31

    IPC分类号: C07D453/02

    摘要: A novel acid addition salt of 3-aminoquinuclidine, which is an industrially useful compound as an intermediate of medicines and does not exhibit deliquescence, is provided. s
    In particular, an acid addition salt of 3-aminoquinuclidine selected from the group consisting of racemic 3-aminoquinuclidine, (R)-3-aminoquinuclidine, and (S)-3-aminoquinuclidine, and acid selected from the group consisting of phosphoric acid, sulfuric acid, fumaric acid, terephthalic acid, oxalic acid, p-toluenesulfonic acid, (±)-10-camphorsulfonic acid, and (-)-10-camphorsulfonic acid, is provided.

    摘要翻译: 提供3-氨基奎宁环的新型酸加成盐,其为工业上有用的化合物作为药物的中间体并且不显示潮解性。 特别地,选自由外消旋3-氨基奎宁环,(R)-3-氨基奎宁环和(S)-3-氨基奎宁环组成的组的3-氨基奎宁环的酸加成盐和选自磷酸 ,硫酸,富马酸,对苯二甲酸,草酸,对甲苯磺酸,(±)-10-樟脑磺酸和( - ) - 10-樟脑磺酸。