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公开(公告)号:EP3334712A1
公开(公告)日:2018-06-20
申请号:EP16745475.0
申请日:2016-08-02
申请人: BASF SE
IPC分类号: C07D231/24 , C07D231/04
CPC分类号: C07D231/22 , C07D231/04 , C07D231/24
摘要: The present invention relates to a process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate (I), comprising a) reacting a compound of formula (II) with an alkylating agent in the presence of a base in the presence of a polar solvent selected from alcohols and ketons; b) the addition of water.
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公开(公告)号:EP3334712B1
公开(公告)日:2019-10-09
申请号:EP16745475.0
申请日:2016-08-02
申请人: BASF SE
IPC分类号: C07D231/24 , C07D231/04
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公开(公告)号:EP2387600A2
公开(公告)日:2011-11-23
申请号:EP09799114.5
申请日:2009-12-28
申请人: BASF SE
发明人: EICHENBERGER, Thomas , RUCH, Thomas , BAUER, Ralf , KREBS, Christoph , LUTERBACHER, Ursula , MAURER, Marc
IPC分类号: C09B57/00 , C07D405/04 , C08K5/00 , C09B67/22
CPC分类号: C09B57/00 , C07D405/04 , C07D493/04 , C08K5/0041 , C09B67/0034 , Y10T428/2982 , Y10T442/30
摘要: A process for preparing a black colorant, preferably a black pigment, characterized in that a compound of the Formula (I) is reacted with a compound of the Formula (II) in a molar ratio of 1:2, in the presence of a catalyst which in water at 25 °C has a pK ≤ 4.5. For the definition of R
1 to R
7 , refer to the description; preferably all are H. Likewise claimed are new crystal polymorphs obtainable by this process, and preferably single-phase mixed crystals. Also claimed are synergistic compositions. These compositions exhibit increased light stability in plastics stabilized with basic light stabilizers when they are pigmented with colorants of the invention rather than with known black pigments such as carbon black. The specification also relates, furthermore, to the use of the black colorants of the invention for coloring paints, printing inks and plastics in the mass, and to mulch film, instrument panels, woven fabrics, garden furniture items or elements for the construction industry that are pigmented with said colorants.-
公开(公告)号:EP2387600B1
公开(公告)日:2014-04-02
申请号:EP09799114.5
申请日:2009-12-28
申请人: BASF SE
发明人: EICHENBERGER, Thomas , RUCH, Thomas , BAUER, Ralf , KREBS, Christoph , LUTERBACHER, Ursula , MAURER, Marc
IPC分类号: C09B57/00 , C07D405/04 , C08K5/00 , C09B67/22
CPC分类号: C09B57/00 , C07D405/04 , C07D493/04 , C08K5/0041 , C09B67/0034 , Y10T428/2982 , Y10T442/30
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