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公开(公告)号：EP2659311B1
公开(公告)日：2017-11-22
申请号：EP11852686.2
申请日：2011-12-15
发明人： TAKAHASHI, Toru , YAMAZAKI, Katsuhisa , MORIBE, Shuhei , YOSHIBA, Daisuke , TSUJIMOTO, Daisuke , FUJIMOTO, Masami
IPC分类号： G03G9/087
CPC分类号： G03G9/08797 , G03G9/0821 , G03G9/0835 , G03G9/08755 , G03G9/08782 , G03G9/08788 , G03G9/08795 , G03G9/0904 , G03G9/091 , G03G9/09783
摘要： To provide a toner that can keep its melt-sticking to sleeve from occurring and, even in double-sided printing, can keep high-temperature offset from occurring and obtain high-quality images on both the surface and the back. The toner comprises toner particles each of which contains a binder resin containing a resin formed by the reaction of i) a resin (A) having a softening point TA (° C.) of 70° C. to 105° C. and having a peak top of endothermic peaks at 55° C. to 120° C. with ii) a resin (B) having a softening point TB (° C.) of 120° C. to 160° C. and having a peak top of endothermic peaks at 55° C. to 120° C., and, in its viscoelasticity characteristics, has a storage elastic modulus at temperature 180° C. (G′180) of 3.0×103 Pa to 3.0×104 Pa, where the loss tangent tan δ has at least one peak having a peak top within the range of 50° C. to 70° C. and, when peak top temperature of the peak is represented by T(° C.), the loss tangent at T+10(° C.) [tan δ(T+10)] is 1.0 to 1.5 and the ratio of tan δ(T+10)/tan δ(110) is 0.8 to 1.5.
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公开(公告)号：EP2659310A1
公开(公告)日：2013-11-06
申请号：EP11852286.1
申请日：2011-12-22
发明人： YAMAZAKI, Katsuhisa , MORIBE, Shuhei , YOSHIBA, Daisuke , TAKAHASHI, Toru , TSUJIMOTO, Daisuke , FUJIMOTO, Masami
CPC分类号： G03G9/087 , G03G9/0821 , G03G9/08755 , G03G9/08795 , G03G9/08797
摘要： A toner is provided which is superior in the long-term storage stability and has high low-temperature fixing properties. In a DSC curve as measured with a differential scanning calorimeter, the toner has a glass transition temperature of not less than 50
o C and not more than 60
o C; and the toner has, in regard to a resin composition contained therein, a difference of not less than 0.060 W/g in heat flow between a point on the curve at a temperature of 40
o C and a baseline in the range exceeding the glass transition temperature; and in viscoelastic characteristics measured at a frequency of 6.28 rad/sec, the toner has a storage elastic modulus (G'40) at a temperature of 40
o C of not less than 7.0 x 10
8 Pa and not more than 2.0 x 10
9 Pa, and a storage elastic modulus (G'70) at a temperature of 70
o C of not less than 1.0 x 10
5 Pa and not more than 1.0 x 10
7 Pa.摘要翻译： 提供长期储存稳定性优异且具有高的低温定影性的调色剂。 在用差示扫描量热计测定的DSC曲线中，调色剂具有不小于50℃且不大于60℃的玻璃化转变温度; 并且调色剂对于其中包含的树脂组合物具有在40℃温度下的曲线上的点与超过玻璃化转变温度的范围内的基线之间的热流动中不小于0.060W / g的差异 ; 并且在以6.28弧度/秒的频率测量的粘弹特性中，调色剂在40℃温度下的储能弹性模量（G'40）不小于7.0×10 8 Pa并且不大于2.0×10 9 Pa ，70℃时的储能弹性模量（G'70）为1.0×10 5 Pa以上且1.0×10 7 Pa以下。
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公开(公告)号：EP4332681A1
公开(公告)日：2024-03-06
申请号：EP22795910.3
申请日：2022-04-28
发明人： MURAYAMA, Ryuji , KITAMURA, Shin , TAKAHASHI, Toru , TSUJIMOTO, Daisuke , MATSUO, Ryuichiro , SANO, Hitoshi , FUJITA, Nobuyuki , YAMADA, Shuji , GUNJI, Yuka , KOBORI, Takakuni , OGAWA, Yoshihiro , OHMORI, Atsuhiko , KAGAWA, Hiroki , ADACHI, Keisuke , SUGITA, Tomoko
IPC分类号： G03G9/097
摘要： The toner is resistant to the generation of toner clumping, exhibits a stable charging performance regardless of the use environment, and exhibits little fluctuation in charging performance even during continuous high-print-count printing. The toner contains binder resin-containing toner particles and silica fine particles S 1, wherein the weight-average particle diameter of the toner is 4.0-15.0 µm, both inclusive. Peaks originating with the silica fine particles S1 are observed in 29 Si-NMR measurement of the silica fine particles S 1, and, in the spectrum obtained by 29 Si CP/MAS NMR or 29 Si DD/MAS NMR, the peak area of a peak corresponding to the D1 unit structure in the silica fine particles S 1, the peak area of a peak corresponding to the D2 unit structure in the silica fine particles S 1, and the peak area of a peak corresponding to the Q unit structure in the silica fine particles S 1 satisfy a prescribed relationship.
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公开(公告)号：EP2659312A1
公开(公告)日：2013-11-06
申请号：EP11854232.3
申请日：2011-12-13
发明人： MORIBE, Syuhei , YAMAZAKI, Katsuhisa , YOSHIBA, Daisuke , TAKAHASHI, Toru , TSUJIMOTO, Daisuke , FUJIMOTO, Masami
IPC分类号： G03G9/087
CPC分类号： G03G9/08755 , G03G9/08702 , G03G9/08788 , G03G9/08797
摘要： A toner comprising toner particles, each of which contains a binder resin and a colorant, wherein the binder resin includes a resin having an endothermic peak at a temperature of 55°C to 120°C in a DSC curve; the toner has a softening point Tm of 90°C to 140°C; in the viscoelastic characteristic of the toner measured at a frequency of 6.28 rad/sec, the storage elastic modulus at a temperature of 180°C is 1.0 × 10
2 Pa to 1.0 × 10
4 Pa; in a chart with the temperature on the x-axis and tanδ on the y-axis, tanδ has a peak having a peak top in the range of 50°C to 70°C; tanδ(P) at the peak top temperature is 2.0 to 10.0; the ratio of the tanδ (P) at the peak top temperature to tanδ (Tm) at a temperature of Tm (tanδ(P) /tanδ (Tm)) is in the range of 2.5 to 8.0.摘要翻译： 一种调色剂，其含有调色剂粒子，所述调色剂粒子各自含有粘合剂树脂和着色剂，所述粘合剂树脂包含在DSC曲线中在55℃〜120℃的温度具有吸热峰的树脂; 该调色剂具有90℃至140℃的软化点Tm; 在以6.28弧度/秒的频率测量的调色剂的粘弹性特性中，在180℃的温度下的储能弹性模量为1.0×10 2 Pa至1.0×10 4 Pa; 在x轴上的温度和y轴上的tanδ的图表中，tanδ具有在50℃至70℃的范围内具有峰顶的峰; tanδ（P）在峰顶温度为2.0-10.0; 温度Tm（tanδ（P）/tanδ（Tm））处的峰顶温度处的tanδ（P）与tanδ（Tm）之比在2.5至8.0的范围内。
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公开(公告)号：EP3617802A1
公开(公告)日：2020-03-04
申请号：EP19193600.4
申请日：2019-08-26
发明人： OHTSU, Takeshi , FUKUDA, Tadashi , AKASAKI, Mikihiro , MIYAMOTO, Akinori , MORI, Kota , HANO, Masami , KASE, Takashi , TSUJIMOTO, Daisuke , MATSUO, Ryuichiro , HOSOI, Kazuto , OGAWA, Yoshihiro
摘要： A toner includes toner particle containing at least a strontium titanate particle on the surface of the toner particle, and the toner is a water-washed toner from which strontium titanate particle desorbable by water washing are removed by water washing. The water-washed toner contains the strontium titanate particle having a number average particle diameter of primary particle (D1) of 10 nm or more and 150 nm or less, and when the distribution of an Sr element in the water-washed toner in the depth direction is determined, (i) the Sr element abundance on the outermost surface x satisfying 0.00
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公开(公告)号：EP2659310B1
公开(公告)日：2017-12-13
申请号：EP11852286.1
申请日：2011-12-22
发明人： YAMAZAKI, Katsuhisa , MORIBE, Shuhei , YOSHIBA, Daisuke , TAKAHASHI, Toru , TSUJIMOTO, Daisuke , FUJIMOTO, Masami
CPC分类号： G03G9/087 , G03G9/0821 , G03G9/08755 , G03G9/08795 , G03G9/08797
摘要： A toner is provided which is superior in the long-term storage stability and has high low-temperature fixing properties. In a DSC curve as measured with a differential scanning calorimeter, the toner has a glass transition temperature of not less than 50° C. and not more than 60° C.; and the toner has, in regard to a resin composition contained therein, a difference of not less than 0.060 W/g in heat flow between a point on the curve at a temperature of 40° C. and a baseline in the range exceeding the glass transition temperature; and in viscoelastic characteristics measured at a frequency of 6.28 rad/sec, the toner has a storage elastic modulus (G′40) at a temperature of 40° C. of not less than 7.0×108 Pa and not more than 2.0×109 Pa, and a storage elastic modulus (G′70) at a temperature of 70° C. of not less than 1.0×105 Pa and not more than 1.0×107 Pa.
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公开(公告)号：EP3486725A1
公开(公告)日：2019-05-22
申请号：EP18206411.3
申请日：2018-11-15
IPC分类号： G03G9/097
摘要： A toner having: a toner particle including a binder resin; and an inorganic fine particle, wherein the inorganic fine particle includes a calcium strontium zirconate fine particle.
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公开(公告)号：EP2671120A1
公开(公告)日：2013-12-11
申请号：EP12742227.7
申请日：2012-02-01
发明人： TAKAHASHI, Toru , YAMAZAKI, Katsuhisa , MORIBE, Shuhei , TSUJIMOTO, Daisuke , IWASAKI, Yosuke , FUJIMOTO, Masami
IPC分类号： G03G9/08
CPC分类号： G03G9/08797 , G03G9/0821 , G03G9/08755 , G03G9/08795
摘要： A toner having toner particles, each of which contains a binder resin and a colorant, wherein in viscoelastic properties of the toner as measured with a rotating flat plate rheometer at a frequency of 6.28 rad/sec: a storage elastic modulus at the temperature of 60° C. (G'60) is in a range from 1.0×107 to 1.0×109 (Pa), and a maximal value (G'p) exists for the storage elastic modulus in a temperature range from 110° C. to 140° C., with this G'p being in a range from 5.0×104 to 5.0×106 (Pa).
摘要翻译： 具有调色剂颗粒的调色剂，每种调色剂颗粒含有粘合剂树脂和着色剂，其中在用旋转平板流变仪以6.28rad / sec的频率测量的调色剂的粘弹性中：在60℃的温度下的储存弹性模量 ℃（G'60）为1.0×10 7〜1.0×10 9（Pa）的范围，在110℃〜140℃的温度范围内的储能弹性模量存在极大值（G'p） ℃，该G'p在5.0×10 4〜5.0×10 6（Pa）的范围内。
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公开(公告)号：EP2659311A1
公开(公告)日：2013-11-06
申请号：EP11852686.2
申请日：2011-12-15
发明人： TAKAHASHI, Toru , YAMAZAKI, Katsuhisa , MORIBE, Shuhei , YOSHIBA, Daisuke , TSUJIMOTO, Daisuke , FUJIMOTO, Masami
IPC分类号： G03G9/087
CPC分类号： G03G9/08797 , G03G9/0821 , G03G9/0835 , G03G9/08755 , G03G9/08782 , G03G9/08788 , G03G9/08795 , G03G9/0904 , G03G9/091 , G03G9/09783
摘要： To provide a toner that can keep its melt-sticking to sleeve from occurring and, even in double-sided printing, can keep high-temperature offset from occurring and obtain high-quality images on both the surface and the back. The toner comprises toner particles each of which contains a binder resin containing a resin formed by the reaction of i) a resin (A) having a softening point TA (°C) of 70°C to 105°C and having a peak top of endothermic peaks at 55°C to 120°C with ii) a resin (B) having a softening point TB (°C) of 120°C to 160°C and having a peak top of endothermic peaks at 55°C to 120°C, and, in its viscoelasticity characteristics, has a storage elastic modulus at temperature 180°C (G'180) of 3.0×10
3 Pa to 3.0×10
4 Pa, where the loss tangent tanδ has at least one peak having a peak top within the range of 50°C to 70°C and, when peak top temperature of the peak is represented by T(°C), the loss tangent at T+10(°C) [tanδ(T+10)] is 1.0 to 1.5 and the ratio of tanδ(T+10)/tanδ(110) is 0.8 to 1.5.摘要翻译： 为了提供能够保持其与套筒不熔融粘附的调色剂，并且即使在双面印刷中，也能够保持高温偏移发生并且在表面和背面获得高质量图像。 所述调色剂包含调色剂颗粒，每种调色剂颗粒含有粘合剂树脂，所述粘合剂树脂包含通过以下反应形成的树脂：i）具有70℃至105℃的软化点TA（℃）并且具有 在55℃至120℃与ii）具有120℃至160℃的软化点TB（℃）且在55℃至120℃具有吸热峰顶部的树脂（B）的吸热峰 C，并且在其粘弹性特性中，在温度180℃（G'180）下的储能弹性模量为3.0×10 3 Pa至3.0×10 4 Pa，其中损耗角正切tanδ具有至少一个具有峰 在T℃10（℃）[tanδ（T + 10）]下的损耗角正切为T℃（℃）时的损耗角正切为50℃〜70℃的范围内，峰的峰顶温度为T 1.0〜1.5，tanδ（T + 10）/tanδ（110）的比例为0.8〜1.5。
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