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公开(公告)号:EP2560946B1
公开(公告)日:2015-10-28
申请号:EP11716771.8
申请日:2011-04-18
IPC分类号: C07C209/86 , C01C1/242 , C07D291/06 , C07C211/05
CPC分类号: C07C209/86 , B01D15/00 , B01D53/58 , B01D2251/50 , B01D2257/406 , C01C1/242 , C07D291/06 , C07C211/05
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公开(公告)号:EP2560919A1
公开(公告)日:2013-02-27
申请号:EP11716770.0
申请日:2011-04-18
IPC分类号: C01C1/242 , C07C209/86 , C07C211/05 , C07D291/06
CPC分类号: C07C209/86 , B01D15/00 , B01D53/58 , B01D2251/50 , B01D2257/406 , C01C1/242 , C07D291/06 , C07C211/05
摘要: The invention relates to a process of producing an ammonium salt composition. The process comprises the steps of providing a process stream comprising sulfuric acid and at least one tertiary amine contacting the process stream with ammonia under conditions effective to form a waste stream and a product stream. The waste stream comprises water, the tertiary amine, and ammonia and the product stream comprises a first amount of ammonium salt. The process further comprises the steps of deriving from the waste stream an off gas stream comprising a preliminary amount of ammonia and contacting the off gas stream with an acid under conditions effective to form an ammonium salt stream and a purge stream. The ammonium salt stream comprises a second amount of ammonium salt and the purge stream comprises a reduced amount of ammonia, which is less than the preliminary amount.
摘要翻译: 本发明涉及生产铵盐组合物的方法。 该方法包括以下步骤:在有效形成废物流和产物流的条件下,提供包含硫酸和至少一种叔胺的工艺物流,所述叔胺使工艺物流与氨接触。 废物流包含水,叔胺和氨,并且产物流包含第一量的铵盐。 该方法进一步包括从废物流得到包含初步量的氨的废气流并在有效形成铵盐流和清洗流的条件下使废气流与酸接触的步骤。 铵盐流包含第二量的铵盐,并且吹扫流包含减少量的氨,其小于初始量。
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公开(公告)号:EP2560946A1
公开(公告)日:2013-02-27
申请号:EP11716771.8
申请日:2011-04-18
IPC分类号: C07C209/86 , C01C1/242 , C07D291/06 , C07C211/05
CPC分类号: C07C209/86 , B01D15/00 , B01D53/58 , B01D2251/50 , B01D2257/406 , C01C1/242 , C07D291/06 , C07C211/05
摘要: The invention relates to a process for producing an ammonium salt composition. The process comprises the steps of providing a process stream comprising sulfuric acid, methylene dichloride, and a tertiary amine or a precursor thereof and contacting the process stream with ammonia under conditions effective to form a product stream and a waste stream. The product stream comprises the ammonium salt and the waste stream comprises water, methylene dichloride, ammonia, and the tertiary amine. The process further comprises the step of deriving from the waste stream an off gas stream comprising ammonia and a first amount of methylene dichloride. The process also comprises the step of contacting at least a portion of the off gas stream or a derivative thereof with an adsorbent under conditions effective to separate at least a portion of the off gas into a methylene dichloride stream comprising methylene dichloride.
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