摘要:
A process is disclosed for the purification of the diamide of oxalic acid obtained by means a process wherein copper catalysts are used, by means of the washing with aqueous solutions of an ammonium salt of an organic or inorganic acid, operating at a pH value comprised within the range of from 2 to 8, and at a temperature comprised within the range of from 40 to 150°C.
摘要:
A method of removing copper from oxamide obtained through a process which involves the use of copper catalysts, by contacting it with an aqueous solution of a suitable complexing agent, which is capable offorming copper-containing water-soluble complexes and imparts to the aqueous solution a pH comprised between 2 and 8, optionally repeating the contacting step and, finally, recovering the purified oxamide by solid-liquid separation techniques. The claimed process affords oxamide containing less than 25 ppm of copper.
摘要:
A method of removing copper from oxamide obtained through a process which involves the use of copper catalysts, by contacting it with an aqueous solution of a suitable complexing agent, which is capable offorming copper-containing water-soluble complexes and imparts to the aqueous solution a pH comprised between 2 and 8, optionally repeating the contacting step and, finally, recovering the purified oxamide by solid-liquid separation techniques. The claimed process affords oxamide containing less than 25 ppm of copper.
摘要:
A process is disclosed for the preparation of oxamide derivatives wherein one or both -NH 2 groups are replaced by primary or secondary amino groups, through reaction of oxamide with a suitably selected amine of formula RR 1 NH wherein R represents a substituted straight or branched (C 2 -C 12 )alkyl radical wherein the substituent(s) or at least one of the substituents is selected from the group consisting of hydroxy, amino, mono-substituted amino, and di-substituted amino, and R' represents hydrogen or an optionally substituted (C 1 -C 6 )alkyl radical; representative oxamide derivatives which can thus be obtained useful as corrosion inhibitors, intermediates for polymers, polymer stabilizers, and slow-release fertilizers, are also described.
摘要:
A stream of raw phenol, outcoming from the process of production of phenol and acetone from cumene, via cumene hydroperoxide, is purified by means of a combination of treatments of distillation and on silico-aluminates treated with acid.
摘要:
A process is disclosed for the purification of the diamide of oxalic acid obtained by means a process wherein copper catalysts are used, by means of the washing with aqueous solutions of an ammonium salt of an organic or inorganic acid, operating at a pH value comprised within the range of from 2 to 8, and at a temperature comprised within the range of from 40 to 150°C.