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    MFI WITH UNUSUAL MORPHOLOGY
    2.
    发明公开
    MFI WITH UNUSUAL MORPHOLOGY 有权
    不寻常的形态MFI

    公开(公告)号：EP2925671A1

    公开(公告)日：2015-10-07

    申请号：EP13789579.3

    申请日：2013-11-14

    申请人： ExxonMobil Chemical Patents Inc.

    发明人： MERTENS, Machteld M. ,  ANTHONIS, Marc H. ,  BONS, Antonie J. ,  ENGELS, Brita ,  MORTIER, Wilfried J. ,  CHENG, Jane C.

    IPC分类号： C01B39/40

    摘要： A method of making a crystalline molecular sieve of MFI framework type, preferably ZSM-5, from a synthesis mixture comprising at least one source of tetravalent element (Y), at least one source of trivalent element (X), at least one source of alkali metal hydroxide (MOH), at least one structure directing; (R) and water, said synthesis mixture having the following molar composition: YO2, (p)X2O3: (q) MOH: (r) R: (s) H2O, wherein (p) is from 0.005 to 0.025, (q) is from 0.05 to 0.5, (r) is from 0.05 to 0.15 and (s) is from 35 to 45, wherein the ratio of the largest dimension (L) to the smallest dimension (S) of each crystal of the molecular sieve product is at least 5, and the smallest dimension (S) is from 20 nm to 200 nm.

    PROCESS FOR PRODUCING PHENOL AND METHYL ETHYL KETONE
    6.
    发明公开
    PROCESS FOR PRODUCING PHENOL AND METHYL ETHYL KETONE 审中-公开
    生产苯酚和甲基乙基酮的方法

    公开(公告)号：EP1984315A1

    公开(公告)日：2008-10-29

    申请号：EP07711514.5

    申请日：2007-02-08

    申请人： ExxonMobil Chemical Patents Inc. ,  Exxonmobil Chemical Limited

    发明人： DAKKA, Jihad M. ,  STANAT, Jon E. ,  BENITEZ, Francisco M. ,  BUCHANAN, John S. ,  CHENG, Jane C. ,  ELKS, Jeffrey T.

    IPC分类号： C07C37/08 ,  C07C39/04 ,  C07C45/53 ,  C07C49/10 ,  C07C2/66 ,  C07C15/02 ,  C07C409/08

    CPC分类号： C07C409/08 ,  C07C37/08 ,  C07C45/53 ,  C07C407/00 ,  C07C49/10 ,  C07C39/04

    摘要： A process for producing phenol and methyl ethyl ketone comprises contacting benzene and a C4 alkylating agent under alkylation conditions and in the presence of an alkylation catalyst comprising at least one molecular sieve of the MCM-22 family to produce an alkylation effluent comprising secbutylbenzene; wherein the contacting is conducted in a plurality of reaction zones and the C4 alkylating agent is supplied to each of the reaction zones. A secbutylbenzene fraction is recovered from the alkylation effluent and comprises at least 95 wt% sec-butylbenzene, less than 100 wt ppm of C8+ olefins, and less than 0.5 wt% of isobutylbenzene and tert-butylbenzene. The sec-butylbenzene fraction is then oxidized to produce sec-butylbenzene hydroperoxide and the hydroperoxide is cleaved to produce phenol and methyl ethyl ketone.

    摘要翻译： 生产苯酚和甲基乙基酮的方法包括在烷基化条件下并且在包含至少一种MCM-22家族的分子筛的烷基化催化剂的存在下使苯和C4烷基化剂接触以产生包含仲丁基苯的烷基化流出物; 其中所述接触在多个反应区中进行，并且所述C4烷基化剂被供应至每个反应区。 从烷基化流出物中回收仲丁基苯馏分，并包含至少95重量％的仲丁基苯，小于100重量ppm的C8 +烯烃和小于0.5重量％的异丁基苯和叔丁基苯。 然后将仲丁基苯馏分氧化生成仲丁基苯氢过氧化物，并将氢过氧化物裂解生成苯酚和甲基乙基酮。