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    PROCESSES FOR SYNTHESIS OF 1,3,3,3-TETRAFLUOROPROPENE
    1.
    发明公开
    PROCESSES FOR SYNTHESIS OF 1,3,3,3-TETRAFLUOROPROPENE 有权
    合成1,3,3,3-四氟丙烯的方法

    公开(公告)号：EP1740521A1

    公开(公告)日：2007-01-10

    申请号：EP05744032.3

    申请日：2005-04-29

    申请人： Honeywell International Inc.

    发明人： TUNG, Hsueh, S. ,  NAIR, Haridasan, K. ,  MUKHOPADHYAY, Sundip ,  VAN DER PUY, Michael ,  MA, Jing Ji

    IPC分类号： C07C21/18 ,  C07C17/269 ,  C07C17/272 ,  C07C17/358

    CPC分类号： C07C17/206 ,  C07C17/00 ,  C07C17/26 ,  C07C17/269 ,  C07C17/272 ,  C07C17/278 ,  C07C21/18

    摘要： Disclosed is a process for the synthesis of 1,3,3,3-tetrafluoropropene which comprises, in one embodiment, reacting a compound of CF3X1 with a compound of CX2H=CHX3, wherein X1, X2, and X3 are each independently selected from the group consisting of fluorine, chlorine, bromine and iodine, to produce a reaction product comprising a compound of CF3CH=CHX3, wherein X3 is as described above; and when X3 is not fluorine, fluorinating the compound to produce 1,3,3,3-tetrafluoropropene. The process in another embodiment comprises preparing tetrafluoropropene comprising thermally cracking one or more compounds capable of producing a reaction mixture which preferably comprises diflurocarbene radicals and vinylidene fluoride, and converting said reaction mixture into -tetrafluoropropene (1,3,3,3-tetrafluoropropene).

    摘要翻译： 公开了合成1,3,3,3-四氟丙烯的方法，在一个实施方案中，其包括使CF 3 X 1的化合物与CX 2 H = CHX 3的化合物反应，其中X 1，X 2和X 3各自独立地选自 由氟，氯，溴和碘组成的基团，以产生包含CF 3 CH = CHX 3的化合物的反应产物，其中X 3如上所述; 并且当X 3不是氟时，氟化该化合物以产生1,3,3,3-四氟丙烯。 在另一个实施方案中的方法包括制备四氟丙烯，包括热裂解一种或多种能够产生反应混合物的化合物，所述反应混合物优选包含二氟卡宾基团和偏二氟乙烯，并且将所述反应混合物转化为四氟丙烯（1,3,3,3-四氟丙烯）。

    LIQUID PHASE CATALYTIC FLUORINATION OF HYDROCHLOROCARBON AND HYDROCHLOROFLUOROCARBON
    4.
    发明授权
    LIQUID PHASE CATALYTIC FLUORINATION OF HYDROCHLOROCARBON AND HYDROCHLOROFLUOROCARBON 失效
    氯氟烃和氢氟碳化合物氯催化液相氟化

    公开(公告)号：EP0938461B1

    公开(公告)日：2001-10-17

    申请号：EP97948216.3

    申请日：1997-11-12

    申请人： Honeywell International Inc.

    发明人： THENAPPAN, Alagappan ,  TUNG, Hsueh, S. ,  BELL, Robert, L.

    IPC分类号： C07C17/20 ,  C07C17/087 ,  C07C19/08

    CPC分类号： C07C17/206 ,  C07C17/00 ,  C07C17/087 ,  Y10S526/906 ,  Y10S526/913 ,  C07C19/08

    摘要： A process for the catalytic fluorination of hydrochlorocarbons and hydrochlorofluorocarbons in the liquid phase. The process is useful for fluorinating hydrochloropropanes, hydrochlorofluoropropanes, hydrochloropropenes and hydrochlorofluoropropenes and most particularly useful for fluorinating 1,1,1,3,3-pentachloropropane to 1,1,1,3,3-pentafluoropropane. Suitable catalysts include (i) a pentavalent molybdenum halide; (ii) à tetravalent tin halide; (iii) a tetravalent titanium halide; (iv) a mixture of a pentavalent tantalum halide with a tetravalent tin halide; (v) a mixture of a pentavalent tantalum halide with a tetravalent titanium halide; (vi) a mixture of a pentavalent niobium halide with a tetravalent tin halide; (vii) a mixture of a pentavalent niobium halide with a tetravalent titanium halide; (viii) a mixture of a pentavalent antimony halide with a tetravalent tin halide; (ix) a mixture of a pentavalent antimony halide with a tetravalent titanium halide; (x) a mixture of a pentavalent molybdenum halide with a tetravalent tin halide; (xi) a mixture of a pentavalent molybdenum halide with a tetravalent titanium halide and (xii) a mixture of a pentavalent antimony halide with a trivalent antimony halide. Products of this process are useful in a variety of applications including solvents, blowing agents, and refrigerants.