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公开(公告)号：EP0322097B1
公开(公告)日：1994-01-05
申请号：EP88310493.7
申请日：1988-11-08
CPC分类号： B01F3/088 , B01F3/0807 , B01F2003/0842 , B01F2215/0057 , B01F2215/0088 , C06B21/0008 , C06B47/145 , Y10S149/11 , Y10S149/112 , Y10S149/113
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公开(公告)号：EP0569162A1
公开(公告)日：1993-11-10
申请号：EP93303109.8
申请日：1993-04-21
摘要： A process for the production of explosives grade ammonium nitrate prill (EGAN) comprises the steps of
(A). producing seed ammonium nitrate prill as substantially monosized prills; and then
(B). fattening using melt/solution of ammonium or mixed nitrates, with drying and thermal treatments, the seed prill in an inclined rotating jacketed pan granulator or a cascade of such pans to produce a final fattened EGAN prill product preferably having at most about 4 mm diameter.摘要翻译： 一种生产炸药级硝酸铵颗粒（EGAN）的方法包括（A）的步骤。 生产种子硝酸铵颗粒作为基本上单一的颗粒; 然后（B）。 使用熔融/溶液的铵或混合硝酸盐进行干燥和热处理，将种子颗粒在倾斜的旋转夹套盘式制粒机或这种盘的级联中以产生最终具有至多约4mm直径的最终育肥EGAN颗粒产品。
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公开(公告)号：EP0403091A3
公开(公告)日：1992-08-12
申请号：EP90305594.5
申请日：1990-05-23
CPC分类号： C06B21/0008 , B01F3/0807 , B01F3/0853 , B01F7/00 , B01F7/0025 , B01F7/0045 , B01F7/16 , B01F2003/0842 , B01F2215/0057 , B01F2215/0088 , C06B47/145
摘要： A method for producing an emulsion explosive comprises introducing a liquid organic fuel phase and an immiscible liquid oxidiser phase into apparatus having a mixer chamber (5), flow constrictor means (8) for introducing the liquid oxidiser phase as an emergent turbulent jet into the chamber to cause its fragmentation into droplets in situ within the chamber, means (10) for introducing the fuel phase into the chamber (5) so that the fuel phase introduced thereby contacts and becomes distributed around the droplets of oxidiser phase as they form to produce emulsion and further providing shear mixing means (12) within the mixing chamber (5) to effect enhancement of the mixing of the chamber contents and thereby to continuously incorporate the fuel phase to produce a more refined emulsion suitable for use as the basis for an explosive system, particularly emulsions of high velocity.
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4.发明授权
公开(公告)号：EP0009875B1
公开(公告)日：1983-07-06
申请号：EP79301753.4
申请日：1979-08-28
发明人： Anderton, Nicholas William Richard , Barker, Derreck Phillips , Ford, Leslie John , Kirk, Frank Alfred , Oliver, Raymond
CPC分类号： C08G63/80 , B01J8/245 , C08G63/42 , C08G63/785
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公开(公告)号：EP0570119B1
公开(公告)日：1997-05-28
申请号：EP93303110.6
申请日：1993-04-21
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公开(公告)号：EP0403091B1
公开(公告)日：1994-06-15
申请号：EP90305594.5
申请日：1990-05-23
CPC分类号： C06B21/0008 , B01F3/0807 , B01F3/0853 , B01F7/00 , B01F7/0025 , B01F7/0045 , B01F7/16 , B01F2003/0842 , B01F2215/0057 , B01F2215/0088 , C06B47/145
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公开(公告)号：EP0322097A1
公开(公告)日：1989-06-28
申请号：EP88310493.7
申请日：1988-11-08
CPC分类号： B01F3/088 , B01F3/0807 , B01F2003/0842 , B01F2215/0057 , B01F2215/0088 , C06B21/0008 , C06B47/145 , Y10S149/11 , Y10S149/112 , Y10S149/113
摘要： Apparatus for producing a multi-phase emulsion explosive from a liquid organic fuel medium and an immiscible liquid oxidiser comprises a mixing chamber 5, flow constrictor means 8.9 for introducing the liquid oxidiser as an emergent turbulent jet to said chamber and causing formation of droplets of said oxidiser in situ within the chamber, means 10 for introducing the fuel medium to said chamber so that the fuel introduced thereby contacts and stabilises the droplets of oxidiser solution as they are formed to maintain same as discrete droplets of oxidiser liquid and thereby provide an emulsion suitable for use as the basis for an explosive system.
摘要翻译： 用于从液体有机燃料介质和不混溶液体氧化器生产多相乳液炸药的装置包括混合室5，流动压缩装置8,9，用于将液体氧化剂作为紧急湍流喷射引入所述室并引起液滴的形成 所述氧化器在所述室内原位，用于将所述燃料介质引入所述室的装置10，使得由此引入的燃料在其形成时接触并稳定氧化剂溶液的液滴，以保持与离子液体的氧化剂液体相同，从而提供 适用于爆炸系统基础的乳液。
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公开(公告)号：EP0589639A3
公开(公告)日：1994-04-27
申请号：EP93307377.7
申请日：1993-09-17
发明人： Chan, Sek Kwan , Kirby, Ian John , Oliver, Raymond
CPC分类号： C06D5/06 , C06B21/0066 , C06B35/00
摘要： Precipitation of fine azide core particles with in-situ coating with suspended tiny oxide particles, followed by concentration of the dilute suspension of these bodies to form a slurry with residual dissolved azide in the liquor, and finally converting the slurry in to solid aggregates of the pyrotechnic bodies by e.g. prilling whereby liquid phase evaporation releases dissolved azide causing the pyrotechnic bodies to be adhered together in to larger aggregates.
摘要翻译： 用悬浮的微小氧化物颗粒原位涂覆沉淀精细叠氮化物核心颗粒，然后浓缩这些物体的稀释悬浮液以在溶液中形成具有残留溶解的叠氮化物的浆液，最后将浆液转化成固体聚集体 烟火体例如 由此液相蒸发释放溶解的叠氮化物，从而使烟火体被粘合在一起形成较大的聚集体。
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公开(公告)号：EP0589639A2
公开(公告)日：1994-03-30
申请号：EP93307377.7
申请日：1993-09-17
发明人： Chan, Sek Kwan , Kirby, Ian John , Oliver, Raymond
CPC分类号： C06D5/06 , C06B21/0066 , C06B35/00
摘要： Precipitation of fine azide core particles with in-situ coating with suspended tiny oxide particles, followed by concentration of the dilute suspension of these bodies to form a slurry with residual dissolved azide in the liquor, and finally converting the slurry in to solid aggregates of the pyrotechnic bodies by e.g. prilling whereby liquid phase evaporation releases dissolved azide causing the pyrotechnic bodies to be adhered together in to larger aggregates.
摘要翻译： 沉淀具有悬浮微小氧化物颗粒的原位涂层的细叠氮化物芯颗粒，随后浓缩这些体的稀释悬浮液，以在液体中形成具有残留的溶解叠氮化物的浆料，最后将浆料转化为固体聚集体 烟火体例如 造粒，其中液相蒸发释放溶解的叠氮化物，导致烟火物体粘附到较大的聚集体上。
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公开(公告)号：EP0570119A1
公开(公告)日：1993-11-18
申请号：EP93303110.6
申请日：1993-04-21
摘要： Explosive grade ammonium nitrate (EGAN) prills are made by a process that comprises the steps of:
a. continuously spraying a 95 to 98% by weight solution/melt of ammonium nitrate (or a mixture of ammonium nitrate and minor proportions of one or more other EGAN - acceptable nitrates) in/with water under spray-head conditions causing the emergent jets to break into cascades of substantially mono-sized droplets;
b. allowing the formed droplets to fall within a vertical duct;
c. continuously feeding a stream of cooling gas upwards through the duct to effect cooling and solidification of the falling droplets and some removal of moisture so as to form substantially mono-sized EGAN prills of up to about 4 mm diameter, and
d. continuously withdrawing the EGAN prills collecting at the base of the duct (such EGAN prills then optionally being further cooled and/or dried in a forced draught regime),
the process being further characterised by intensification of the upward gas flow regime in the duct such that:
(i) the temperature difference of the gas flow between its inlet to the duct and its outlet from the duct is at least about 60°C; and
(ii) the falling velocity of the prills in the duct is at most about 3 metres/second relative to ground (i.e. a stationary observer external to the duct) the upward gas flow velocity being e.g. 6 m/s relative to ground for 2 mm prill and 9 m/s for 3 mm prill and, optionally,
(iii) recycling the gas stream after washing and cooling and addition of any required make-up gas.摘要翻译： 爆炸级硝酸铵（EGAN）颗粒通过包括以下步骤的方法制备：a。 在喷头条件下在水中连续喷洒95-98重量％的硝酸铵溶液/熔融物（或硝酸铵与少量一种或多种其他EGAN-可接受的硝酸盐的混合物），导致急流喷射破裂 分成基本上单一尺寸的小滴的级联; 湾 使形成的液滴落入垂直管道内; C。 通过管道向上连续输送冷却气体流以实现降落液滴的冷却和固化以及一些水分的去除，从而形成直径高达约4mm的基本上单尺寸的EGAN颗粒，以及d。 连续地收回在管道底部收集的EGAN颗粒（这种EGAN颗粒随后任选地在强制通风制度下被进一步冷却和/或干燥），该方法的进一步特征在于强化管道中的向上气流状态，使得 ：（i）其进入管道的入口与其离开管道的出口之间的气流温度差至少约为60℃; 和（ii）管道中的颗粒的下降速度相对于地面（即管道外部的静止观察者）至多约3米/秒，向上的气体流速为例如， 对于2mm颗粒为6m / s，对于3mm颗粒为9m / s，并且任选地，（iii）在洗涤和冷却后再循环气流并添加任何所需的补充气体。
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