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1.发明公开GLOBULAR RUBBER ADJUVANTS AND THE METHOD OF PREPARATING THE SAME 有权VERFAHREN ZUR HERSTELLUNG VONGLOBULÄRENKAUTSCHUKADJUVANTIEN
公开(公告)号：EP2085135A1
公开(公告)日：2009-08-05
申请号：EP07816567.7
申请日：2007-10-15
发明人： WANG, Nongyue , MAO, Xiaohui , FENG, Xiaogen , CHENG, Qianwen , WANG, Luxin
CPC分类号： B29B9/12 , B29B9/10 , B29K2021/00
摘要： The present invention provides spherical rubber chemicals and the method for preparing the same. The spherical rubber chemicals of the present invention include spherical antioxidants, spherical vulcanization agents, spherical processing aids, spherical reinforcing agents, or spherical adhesive agents. With the spherical rubber chemicals of the present invention, the shortcomings of powdery or semi-spherical rubber chemicals are overcome, including eliminating the dust pollution during granulation procedure and avoiding the raw material loss and the environmental pollution, while solving the quality problem of lower melting point of product caused by the presence of fine powder crystal. Furthermore, the resultant rubber chemicals has an improved smoothness of surface, which is helpful to improve the flowing and mixing behaviors of the rubber chemicals in mixing or open milling process with rubbers.
摘要翻译： 本发明提供球形橡胶化学品及其制备方法。 本发明的球形橡胶化学品包括球形抗氧化剂，球形硫化剂，球形加工助剂，球形增强剂或球形粘合剂。 对于本发明的球形橡胶化学品，克服了粉状或半球形橡胶化学品的缺点，包括消除造粒过程中的粉尘污染，避免原料损失和环境污染，同时解决低熔点的质量问题 由于细粉晶体的存在引起的产品点。 此外，所得到的橡胶化学品具有改善的表面平滑度，这有助于改善橡胶化学品在与橡胶混合或开放研磨过程中的流动和混合行为。
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公开(公告)号：EP2085135B1
公开(公告)日：2013-02-13
申请号：EP07816567.7
申请日：2007-10-15
发明人： WANG, Nongyue , MAO, Xiaohui , FENG, Xiaogen , CHENG, Qianwen , WANG, Luxin
CPC分类号： B29B9/12 , B29B9/10 , B29K2021/00
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公开(公告)号：EP1645555B1
公开(公告)日：2011-09-28
申请号：EP04738332.8
申请日：2004-07-02
发明人： WANG, Nongyue , YU, Ruibiao , MAO, Xiaohui , FENG, Xiaogen , CHENG, Qianwen
IPC分类号： C07C211/55 , C07C209/36 , C07C209/60
CPC分类号： C07C211/55 , C07C209/36 , C07C209/60 , Y02P20/584
摘要： The present invention discloses a method for producing 4-aminodiphenylamine by reacting nitrobenzene with a aniline in the presence of complex base catalyst for condensation and complex powdery catalyst for hydrogenation, which comprises the steps of condensation, separation, hydrogenation, separation II and refining sequentially. The method of the present invention can be carried out continuously. By using the complex base catalyst for the condensation, followed being separated and recycling before the hydrogenation, the problem of heat-sensitive decomposition of the complex base catalyst during the hydrogenation procedure can be avoided. Accordingly, the choice of the hydrogenation catalyst is increased, and lower-cost hydrogenation catalysts can be used. Meanwhile, the apparatus can be selected easily and the industrialization can be achieved simply. The complex base catalyst according to the invention is cheaper. The catalystic activity of the catalyst is high and the condition of the reaction is gentle. Additionally, the complex base catalyst is suitable to a wide range of water content. Accordingly the amount of the by-product is decreased, and the conversion and the selectivity can be increased. The labour intensity of the process control is low. Moreover, corrodible liquid is not generated and the environmental pollution can be reduced. The content of 4aminodiphenylamine reaches 99% (by weigh), and yield of the industrial- scale production is greater than 95%.
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