公开(公告)号：EP2290356A2

公开(公告)日：2011-03-02

申请号：EP10189959.9

申请日：2006-02-10

申请人： PerkinElmer LAS, Inc.

发明人： Schick, Christoph

IPC分类号： G01N25/48 ,  G01K17/08

CPC分类号： G01K17/00 ,  G01N25/4866

摘要： The invention relates to calorimetric analytical instruments, and more particularly to a differential scanning calorimeter (100), comprising a sample cell (10), a reference cell (8), a first thermal shield (24) adjacently positioned to the sample cell (10), a second thermal shield (24) adjacently positioned to the reference cell (8), at least one heating system capable of heating said sample cell (10), said reference cell (8), said first thermal shield (24) and said second thermal shield (24), and a temperature monitoring device which monitors a temperature differential between the sample cell (10) and the reference cell (8). The temperature of the shields (24) is controlled such that baseline curvature is reduced by eliminating heat flow from the furnaces to their surroundings (quasi adiabatic conditions) and by controlling heat flow through a well defined solid state heat resistance between the furnaces and a temperature controlled heat sink.

摘要翻译： 本发明涉及量热分析仪器，更具体地涉及一种差示扫描量热计（100），其包括样品池（10），参考单元（8），相邻定位于样品室（10）的第一热屏蔽 ，相邻地定位到参考单元（8）的第二热屏蔽（24），至少一个能够加热所述样品池（10），所述参考单元（8），所述第一热屏蔽（24）和所述第一热屏蔽 第二热屏蔽（24），以及监测样品池（10）和参考单元（8）之间的温度差的温度监测装置。 控制屏蔽件（24）的温度，以便通过消除从炉子到其周围环境的热流（准绝热条件）并且通过控制热流通过熔炉之间良好定义的固态耐热性和温度 受控散热器。