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公开(公告)号:EP2279161A4
公开(公告)日:2014-08-20
申请号:EP08874045
申请日:2008-09-01
申请人: RELIANCE IND LTD
发明人: GUPTA VIRENDRAKUMAR , SINGH SAURABH , MAKWANA UMESH , JOSEPH JOMICHAN , SINGALA KAMLESH , RAJESH SMITHA , PATEL VALLABHBHAI , YADAV MUKESHKUMAR , SINGH GURMEET
CPC分类号: C07C31/28 , C07C29/70 , C08F10/00 , C07C31/30 , C08F4/6494 , C08F4/6548
摘要: The invention relates to a process for the synthesis of spheroidal magnesium alkoxide having improved mechanical strength and narrow particle size distribution, the process comprising reacting magnesium metal, in the presence of iodine, with a mixture of alcohols by step-wise heating first in the range of 40° C. to 65° C. for a period of 2 hours and then in the range of 65° C. to 80° C. for a period of 1 hour, further by maintaining reaction temperature at 80° C. for a period of 6-10 hours, the vapors of the mixture produced during the reaction being condensed in an overhead condenser, hydrogen gas produced during the reaction being vented off and the mixture of alcohols left after the reaction being filtered and reused. The invention also relates to spheroidal magnesium alkoxide particles synthesized by the method, to the Ziegler natta procatalyst synthesized by using the alkoxide and to the polymer resin synthesized using the procatalyst.