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1.发明公开SOLID SOLUTION MATERIAL OF RARE EARTH ELEMENT FLUORIDE (POLYCRYSTAL AND SINGLE CRYSTAL), AND METHOD FOR PREPARATION THEREOF, AND RADIATION DETECTOR AND TEST DEVICE 有权混合晶体材料SELTENERDELEMENTFLUORID用于生产和辐射探测器和测试设备（多晶和单晶）和process
公开(公告)号：EP1754808A4
公开(公告)日：2009-06-17
申请号：EP05730595
申请日：2005-04-12
发明人： YOSHIKAWA AKIRA , AOKI KENJI , SATONAGA TOMOHIKO , KAMADA KEI , FUKUDA TSUGUO
IPC分类号： C30B29/12 , C09K11/00 , C09K11/08 , C09K11/77 , C09K11/85 , G01T1/20 , G01T1/202 , G21K4/00 , H01S3/16
CPC分类号： C09K11/7719 , C09K11/7772 , C30B29/12 , G21K4/00
摘要： A solid solution material of rare earth element fluoride (a polycrystl and/or a single crystal), characterized in that it comprises a combination of a plurality of rare earth element fluorides exhibiting phase transition and having different ionic radii and has no phase transition; a rare earth element fluoride solid solution material (a polycrystl and/or a single crystal), characterized in that it is represented by (REyRE'1-y)F3 (0.0000
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2.发明公开Pr-CONTAINING SINGLE CRYSTAL FOR SCINTILLATOR, PROCESS FOR PRODUCING THE SAME, RADIATION DETECTOR AND INSPECTION APPARATUS 审中-公开PR-含单晶FOR闪烁工艺制作，辐射探测器和检查设备
公开(公告)号：EP1816241A4
公开(公告)日：2010-04-28
申请号：EP05800432
申请日：2005-11-07
发明人： YOSHIKAWA AKIRA , OGINO HIRAKU , KAMADA KEI , AOKI KENJI , FUKUDA TSUGUO
IPC分类号： C30B29/28 , C09K11/00 , C09K11/08 , C09K11/78 , C09K11/79 , C09K11/80 , C30B11/04 , G01T1/20 , G01T1/202
CPC分类号： C30B15/08 , C09K11/7774 , C30B29/22 , C30B29/28 , C30B29/34 , G01T1/1644 , G01T1/2985 , G21K4/00
摘要： The present invention provides an oxide-base scintillator single crystal having an extremely large energy of light emission, adoptable to X-ray CT and radioactive ray transmission inspection apparatus, and more specifically to provide a Pr-containing, garnet-type oxide single crystal, a Pr-containing perovskite-type oxide single crystal, and a Pr-containing silicate oxide single crystal allowing detection therefrom light emission supposedly ascribable to 5d-4f transition of Pr.
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3.发明公开
公开(公告)号：EP1734005A4
公开(公告)日：2008-01-23
申请号：EP05720635
申请日：2005-03-11
申请人： STELLA CHEMIFA CORP
CPC分类号： C01G33/00 , C01G35/00 , C01P2004/03 , C01P2004/10
摘要： A method for preparing tantalum oxide and/or niobium oxide, characterized in that it comprises adding a basic aqueous solution to an aqueous solution of tantalum fluoride salt and/or niobium fluoride salt, to form tantalum hydroxide and/or niobium hydroxide, and then firing said tantalum hydroxide and/or niobium hydroxide. The above method allows the preparation of the tantalum oxide and/or niobium oxide in the state of a needle crystal or columnar crystal, not of a spherical crystal or an assemblage form.
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公开(公告)号：EP2123601A4
公开(公告)日：2012-04-04
申请号：EP08704433
申请日：2008-02-05
申请人： STELLA CHEMIFA CORP
发明人： WAKI MASAHIDE , MIYAMOTO KAZUHIRO , AOKI KENJI
IPC分类号： C01B25/455 , C01B13/00 , C01D13/00 , C01D15/00
CPC分类号： C01D15/005 , C01B25/455 , C01D13/00
摘要： In the manufacturing method of hexafluorophosphate (MPF 6 : M = Li, Na, K, Rb, Cs, NH 4 , and Ag) of the present invention, at least a H x PO y F z aqueous solution, a hydrofluoric acid aqueous solution, and MF · r (HF) are used as raw materials (wherein, r ‰¥ 0, 0 ‰¤ x ‰¤ 3, 0 ‰¤ y ‰¤ 4, and 0 ‰¤ z ‰¤ 6). According to the above description, a manufacturing method of hexafluorophosphate can be provided which is capable of manufacturing hexafluorophosphate (GPF 6 : G = Li, Na, K, Rb, Cs, NH 4 , and Ag) at a low cost in which the raw materials can be easily obtained, the control of the reaction is possible, and the workability is excellent.
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5.发明公开
公开(公告)号：EP2123600A4
公开(公告)日：2012-04-11
申请号：EP08704434
申请日：2008-02-05
申请人： STELLA CHEMIFA CORP
发明人： WAKI MASAHIDE , MIYAMOTO KAZUHIRO , AOKI KENJI
CPC分类号： C01B25/10 , C01B25/455 , C01D15/005
摘要： A process for phosphorus pentafluoride production by which high-purity phosphorus pentafluoride can be produced by a simple and economical procedure without the need of a large-scale purification apparatus or high-pressure apparatus and without generating a large amount of a by-product gas requiring a special discharge-gas treatment. The process for phosphorus pentafluoride production is characterized by introducing hydrogen fluoride and a hexafluorophosphate (MPF 6 ) into a vessel and reacting them according to the reaction shown by the scheme (1) to yield phosphorus pentafluoride. MPF 6 + uHF †’ PF 5 + MF r(HF) (Scheme 1) In the scheme, M is at least any one of Li, Na, K, Rb, Cs, NH 4 , and Ag; 0 ‰¤ r ‰¤ u; and the HF is used in an amount not smaller than the stoichiometric amount.
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