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    Method for preparing monohalogenosilanes
    2.
    发明公开
    Method for preparing monohalogenosilanes 失效
    制备单烯基苯偶姻的方法

    公开(公告)号：EP0461597A3

    公开(公告)日：1992-05-13

    申请号：EP91109515.6

    申请日：1991-06-10

    申请人： Shin-Etsu Chemical Co., Ltd.

    发明人： Kubota, Tohru, SHIN-ETSU CHEMICAL CO., LTD. ,  Kurosaki, Tadao, SHIN-ETSU CHEMICAL CO., LTD. ,  Ishihara, Toshinobu, SHIN-ETSU CHEMICAL CO., LTD. ,  Endo, Mikio, SHIN-ETSU CHEMICAL CO., LTD.

    IPC分类号： C07F7/12

    CPC分类号： C07F7/123

    摘要： This invention relates to a method for preparing a monohalogenosilane, R¹R²R³SiX which comprises the step of subjecting, to a rearrangement reaction, an organodisiloxane, (R¹R²R³Si)₂O and a polyhalogenosilane, R⁴ n SiX 4-n in the presence of active carbon or an ammonium salt, R⁵R⁶R⁷R⁸NY as a catalyst (wherein R¹, R², R³ and R⁸ each represents a hydrogen atoms or a monovalent hydrocarbon group; R⁴, R⁵, R⁶ and R⁷ each represents a monovalent hydrocarbon group, a part or whole of the hydrogen atoms in each hydrocarbon group may be substituted with other atoms or groups; X represents a halogen atom; Y represents a monovalent anion; n is 0, 1 or 2). The method permits the easy preparation of monohalogenosilanes, in a high yield, which are useful as starting materials for use in making silylating agents as well as a variety of organosilicon compounds without using any harmful hexaalkylphosphoric acid triamide type catalyst.

    Method for preparing monohalogenosilanes
    3.
    发明公开
    Method for preparing monohalogenosilanes 失效
    Verfahren zur Herstellung von Monohalogenosilanen。

    公开(公告)号：EP0461597A2

    公开(公告)日：1991-12-18

    申请号：EP91109515.6

    申请日：1991-06-10

    申请人： Shin-Etsu Chemical Co., Ltd.

    发明人： Kubota, Tohru, SHIN-ETSU CHEMICAL CO., LTD. ,  Kurosaki, Tadao, SHIN-ETSU CHEMICAL CO., LTD. ,  Ishihara, Toshinobu, SHIN-ETSU CHEMICAL CO., LTD. ,  Endo, Mikio, SHIN-ETSU CHEMICAL CO., LTD.

    IPC分类号： C07F7/12

    CPC分类号： C07F7/123

    摘要： This invention relates to a method for preparing a monohalogenosilane, R¹R²R³SiX which comprises the step of subjecting, to a rearrangement reaction, an organodisiloxane, (R¹R²R³Si)₂O and a polyhalogenosilane, R⁴ n SiX 4-n in the presence of active carbon or an ammonium salt, R⁵R⁶R⁷R⁸NY as a catalyst (wherein R¹, R², R³ and R⁸ each represents a hydrogen atoms or a monovalent hydrocarbon group; R⁴, R⁵, R⁶ and R⁷ each represents a monovalent hydrocarbon group, a part or whole of the hydrogen atoms in each hydrocarbon group may be substituted with other atoms or groups; X represents a halogen atom; Y represents a monovalent anion; n is 0, 1 or 2). The method permits the easy preparation of monohalogenosilanes, in a high yield, which are useful as starting materials for use in making silylating agents as well as a variety of organosilicon compounds without using any harmful hexaalkylphosphoric acid triamide type catalyst.

    摘要翻译： 本发明涉及制备单卤代硅烷，R 1 R 2 R 3 SiX的方法，该方法包括使有机二硅氧烷（R 1 R 2 R 3） 3 Si）2 O和多卤代硅烷，R 4 nSiX 4-n在活性碳或铵盐的存在下作为催化剂（其中R 5 R 6 R 7 R 8 NY） R 1，R 2，R 3和R 8各自表示氢原子或一价烃基; R 4，R 5，R 6和R 7各自表示 每个烃基中的一价烃基，一部分或全部氢原子可以被其它原子或基团取代; X表示卤素原子; Y表示一价阴离子; n表示0,1或2）。 该方法允许以高产率容易地制备单卤代硅烷，其可用作制备甲硅烷基化试剂的原料以及各种有机硅化合物，而不使用任何有害的六烷基磷酸三酰胺型催化剂。