METHOD FOR PRODUCING DIFLUOROPHOSPHATE
    1.
    发明公开
    METHOD FOR PRODUCING DIFLUOROPHOSPHATE 有权
    生产二氟磷酸酯的方法

    公开(公告)号:EP2826747A1

    公开(公告)日:2015-01-21

    申请号:EP12871541.4

    申请日:2012-03-14

    IPC分类号: C01B25/455

    摘要: A process for preparing difluorophosphate comprising reacting difluorophosphoric acid with at least one salt, as a raw material, selected from a halide salt, a carbonate, a phosphate, a hydroxide and an oxide of an alkali metal, an alkaline earth metal or an onium in the difluoraphosphoric acid, then separating a precipitate from the difluorophosphoric acid by solid-liquid separation, the precipitate being precipitated by crystallization operation in the difluorophosphoric acid, and removing the difluorophosphoric acid contained in the precipitate by distillation to obtain difluorophosphate.

    摘要翻译: 一种二氟磷酸盐的制造方法,其特征在于,使二氟磷酸与选自碱金属的卤化物盐,碳酸盐,磷酸盐,氢氧化物和氧化物中的至少一种以上的盐作为原料, 然后通过固液分离从二氟磷酸中分离析出物,通过在二氟磷酸中的结晶操作使析出物析出,通过蒸馏除去析出物中含有的二氟磷酸,得到二氟磷酸盐。