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    Method and apparatus for electrothermal atomization of samples
    2.
    发明公开
    Method and apparatus for electrothermal atomization of samples 失效
    Verfahren und Vorrichtung zur elektrothermischen Atomisierung von Proben。

    公开(公告)号：EP0356566A1

    公开(公告)日：1990-03-07

    申请号：EP88114360.6

    申请日：1988-09-02

    申请人： THE PERKIN-ELMER CORPORATION

    发明人： de Loos-Vollebregt, Margaretha T C ,  Bank, Petrus C ,  de Galan, Leo

    IPC分类号： G01N21/74 ,  G01N1/00

    CPC分类号： G01N21/74 ,  G01N1/22

    摘要： Sample liquid is vaporized by a thermospray vaporizer (24) with a heated capillary tube (36). The end of the capillary tube (36) is inserted into a graphite tube furnace (120), while the furnace and a vertical platform in this furnace is at an above-ambient deposition temperature. The vavor spray emerging from the capillary tube is directed towards the platform. Sample substances are deposited on the platform, while vaporized solvent is drawn off by a vacuum. Larger quantities of sample without the solvent can be deposited in this way on a small platform. This permits using the platform technique without the limitations as to the quantity of the sample normally inherent with this technique.

    摘要翻译： 用热喷雾蒸发器（24）用加热的毛细管（36）将样品液体汽化。 毛细管（36）的末端插入石墨管式炉（120）中，炉子和炉内的垂直平台处于高于环境的沉积温度。 从毛细管出现的气味喷雾指向平台。 样品物质沉积在平台上，而蒸发的溶剂则被抽真空。 没有溶剂的较大量的样品可以以这种方式沉积在小平台上。 这允许使用平台技术，而不受对该技术通常固有的样本量的限制。