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    Method for sulfonating acyloxybenzenes and neutralization of resulting product
    1.
    发明公开
    Method for sulfonating acyloxybenzenes and neutralization of resulting product 失效
    Verfahren zur Sulfonierung von Acyloxybenzolen und zur Neutralisierung der resultierenden Produkte。

    公开(公告)号：EP0506308A1

    公开(公告)日：1992-09-30

    申请号：EP92302417.8

    申请日：1992-03-20

    申请人： The Clorox Company

    发明人： Ottoboni, Thomas B. ,  Zielske, Alfred G. ,  Kuhner, Lisa M. ,  Brodbeck, Kevin J. ,  Sinisi, Leonardo ,  Martin, Gregory T. ,  Spillett, Cris Tina ,  Thompson, Suzanne M. ,  Steichen, Dale S.

    IPC分类号： C07C309/42 ,  C07C303/32 ,  C07C303/06

    CPC分类号： C11D3/3907 ,  C07C303/06 ,  C07C303/32 ,  C07C309/42

    摘要： A method is provided for sulfonating an acyloxy substituted benzene ring to obtain high yields of desired sulfonated compounds that are useful as cleaning, bleaching, or fabric treating additives. A particularly preferred additive so prepared has the structure

    where R⁷ is a branched or unbranched alkyl with about 5 to 9 carbons and M is an alkali metal, an alkaline earth metal, or ammonium. The benzene ring is sulfonated by contacting with a molar excess of sulfur trioxide source and then irreversibly reacting the sulfur trioxide excess with a quenching agent. A neutralization process for preparing peracid precursors in high yield by neutralizing sulfonated aryl esters is also provided.

    摘要翻译： 提供了用于磺化酰氧取代的苯环以获得高产率的用作清洁，漂白或织物处理添加剂的所需磺化化合物的方法。 如此制备的特别优选的添加剂具有结构，其中R 7是具有约5至9个碳的支链或非支链烷基，M是碱金属，碱土金属或铵。 苯环通过与摩尔过量的三氧化硫源接触而磺化，然后使三氧化硫过氧化物与猝灭剂不可逆地反应。 还提供了通过中和磺化芳基酯以高产率制备过酸前体的中和方法。