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1.发明授权POSITIVE ELECTRODE ACTIVE MATERIAL GRANULAR POWDER AND METHOD FOR PRODUCING SAME, AND NONAQUEOUS ELECTROLYTE SECONDARY BATTERY 有权粒状粉末作为正极活性物质，工艺用于生产和二次电池的非水电解质
公开(公告)号：EP2693535B1
公开(公告)日：2016-08-31
申请号：EP12763014.3
申请日：2012-03-22
CPC分类号： C01D15/02 , C01G53/50 , C01P2002/52 , C01P2002/72 , C01P2002/74 , H01M4/505 , H01M4/525 , Y02E60/122 , Y02P70/54
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2.发明公开POSITIVE ELECTRODE ACTIVE MATERIAL GRANULAR POWDER AND METHOD FOR PRODUCING SAME, AND NONAQUEOUS ELECTROLYTE SECONDARY BATTERY 有权粒状粉末作为正极活性物质，工艺用于生产和二次电池的非水电解质
公开(公告)号：EP2693535A1
公开(公告)日：2014-02-05
申请号：EP12763014.3
申请日：2012-03-22
CPC分类号： C01D15/02 , C01G53/50 , C01P2002/52 , C01P2002/72 , C01P2002/74 , H01M4/505 , H01M4/525 , Y02E60/122 , Y02P70/54
摘要： The present invention provides positive electrode active substance particles which are improved in charge/discharge capacities, cycle characteristics and thermal stability. The positive electrode active substance particles according to the present invention comprise a compound having at least a crystal system belonging to a space group of R-3m and a crystal system belonging to a space group of C2/m and having a specific peak intensity ratio, in which a content of Mn in the compound is controlled such that a molar ratio of Mn/(Ni + Co + Mn) therein is not less than 0.55; a content of boron in the compound is 0.01 to 1% by weight; a content of fluorine in the compound is 0.01 to 5% by weight; and a content of an element A (at least one element selected from the group consisting of Al, Mg, Ti, Zr, Ca, Fe, Zn, Mo and Bi) in the compound is 0.004 to 9% by weight, and can be produced by calcining a mixture comprising precursor particles comprising Mn and Ni and/or Co, a lithium compound, a boron compound, a fluorine compound and a compound of the element A.
摘要翻译： 本发明提供作为在充电/放电容量，循环特性和热稳定性改进的正极活性物质粒子。 另外，正极活性物质粒子雅丁到，本发明包含具有化合物至少属于空间群R-3m的和属于空间群C2 / m的晶体系统和具有特定峰强度比的晶系， 中的Mn的化合物中的一个内容被控制搜索那样的Mn /（镍+钴+ Mn）的摩尔比。其中不小于0:55少; 硼的化合物的含量为0时01〜1重量％; 按重量计的氟化合物中的含量为0时01％至5％; 和元素A的化合物（选自铝，镁，钛，锆，钙，铁，锌，钼和铋由......组成中选择的至少一种元素）的含量为0.004％至9％（重量），并且可以是 通过煅烧包含含有Mn和Ni和/或Co，锂化合物，硼化合物，氟化合物和元素A的化合物的前体颗粒的混合物生产
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3.发明公开OXYCOBALT HYDROXIDE PARTICULATE POWDER AND MANUFACTURING METHOD THEREFOR, AS WELL AS LITHIUM COBALTATE PARTICULATE POWDER, MANUFACTURING METHOD THEREFOR, AND NON-AQUEOUS ELECTROLYTE SECONDARY BATTERY USING THE SAME 有权用于生产和粒子状的钴酸锂，用于生产和二次电池的非水电解液使用其粒子状OXYCOBALTHYDROXIDPULVER AND PROCESS
公开(公告)号：EP2314545A1
公开(公告)日：2011-04-27
申请号：EP09725552.5
申请日：2009-03-26
发明人： KOBINO, Masashi , FUJITA, Katsuhiro , OKAZAKI, Seiji , HONDA, Tomohiro , NISHIO, Takahisa , FUJIMOTO, Ryota , HIRAMOTO, Toshiaki , SATO, Kouta , ITO, Akino , OKINAKA, Kenji , FUJINO, Shoichi , NISHIMOTO, Kazushi , UEGAMI, Masayuki , MORITA, Daisuke , KAJIYAMA, Akihisa
CPC分类号： C01G51/04 , C01G51/42 , C01P2002/52 , C01P2002/60 , C01P2002/72 , C01P2002/88 , C01P2004/03 , C01P2004/51 , C01P2004/61 , C01P2004/62 , C01P2006/10 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/131 , H01M4/1391 , H01M4/485 , H01M4/525 , H01M10/052
摘要： The present invention relates to cobalt oxyhydroxide particles and lithium cobaltate particles which have a high density and a uniformly grown crystal structure. These objects of the present invention can be achieved by cobalt oxyhydroxide particles having an average secondary particle diameter (D50) of 3.0 to 25.0 µm, a BET specific surface area (BET) of 0.1 to 20.0 m 2 /g, a tap density (TD) of 1.0 to 3.5 g/cm 3 in which the average secondary particle diameter (D50) and the BET specific surface area (BET) of the cobalt oxyhydroxide particles satisfy the relational formula; and by lithium cobaltate particles having an average secondary particle diameter (D50) of 15.0 to 25.0 µm, a specific surface area (BET) of 0.10 to 0.30 m 2 /g, a compressed density (CD; as measured by applying a pressure of 2.5 t/cm 2 thereto) of 3.65 to 4.00 g/cm 3 . The cobalt oxyhydroxide particles are useful as a precursor of a positive electrode active substance (lithium cobaltate particles) used in a non-aqueous electrolyte secondary battery, and the lithium cobaltate particles are useful as a the positive electrode active substance used in a non-aqueous electrolyte secondary battery.
摘要翻译： 本发明涉及到碱式氢氧化钴的颗粒和钴酸锂具有高密度和均匀地生长晶体结构的粒子。 本发明的这些目的可以通过具有上的0.1 3.0至25.0微米，BET比表面积（BET）平均二次粒径（D50）氢氧化正钴颗粒取得〜20.0米2 /克，堆积密度（TD ）的1.0〜3.5克/厘米3，其中，平均二次粒径（D50）和氢氧化正钴颗粒的BET比表面积（BET）满足关系式; 和由钴酸锂颗粒，其具有上的12:10 15.0至25.0微米，比表面积（BET）平均二次粒径（D50）为00:30米2 /克，压缩密度（CD;通过施加2.5的压力测量 吨/ 3.65至4.00克/立方厘米厘米2于此）。 氢氧化正钴颗粒是作为在非水电解质二次电池中使用的正极活性物质（钴酸锂粒子）的前体是有用的，且钴酸锂颗粒是作为非水使用的正极活性物质有用的 电解质二次电池。
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4.发明公开
公开(公告)号：EP2277828A1
公开(公告)日：2011-01-26
申请号：EP09727078.9
申请日：2009-03-26
发明人： MISHIMA, Yuji , HONDA, Shingo , KONO, Yoshiteru , SATO, Kouta , OKAZAKI, Seiji , KATAMOTO, Tsutomu
CPC分类号： H01M4/5825 , C01B25/45
摘要： The present invention relates to a process for producing lithium iron phosphate particles having an olivine type structure, comprising a first step of mixing an iron oxide or an iron oxide hydroxide as an iron raw material which comprises at least one element selected from the group consisting of Na, Mg, Al, Si, Cr, Mn and Ni in an amount of 0.1 to 2 mol% for each element based on Fe, and a carbon element C in an amount of 5 to 10 mol% based on Fe, and has a content of Fe 2+ of not more than 40 mol% based on an amount of Fe and an average primary particle diameter of 5 to 300 nm, with a lithium raw material and a phosphorus raw material; a second step of controlling agglomerates diameter in the resulting mixture is 0.3 to 5.0 µm; and a third step of sintering the mixture obtained in the second step in an inert gas or reducing gas atmosphere having an oxygen concentration of not more than 0.1% at a temperature of 250 to 750°C.
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