Alkylation of substituted sulfonylpyridine 1-oxides
    1.
    发明公开
    Alkylation of substituted sulfonylpyridine 1-oxides 失效
    取代的磺酰基吡啶1-氧化物的烷基化。

    公开(公告)号:EP0073592A1

    公开(公告)日:1983-03-09

    申请号:EP82304300.5

    申请日:1982-08-13

    申请人: UNIROYAL, INC.

    CPC分类号: C07D213/89 C07D213/71

    摘要: Making a compound of the formula
    wherein:

    R is C 1 -C 12 alkyl, allyl or benzyl,
    R 1 and R 2 are hydrogen, halogen, C 1 -C 4 alkyl, or phenyl,
    R 3 is hydrogen, halogen, C 1 -C 4 alkyl, C 1 -C 4 alkoxy, CF 3 , N0 2 , phenyl or phenoxy, m is an integer from 1 to 3 and
    n is zero or 1, by contacting a compound of said formula where R is hydrogen with certain halohydrocarbons in the presence of solid KOH, a phase transfer catalyst, a solvent and an effective amount of water.