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公开(公告)号：EP3971135A1
公开(公告)日：2022-03-23
申请号：EP19942869.9
申请日：2019-09-02
发明人： DONG, Chao , ZHAO, Dongke , ZHOU, Yujie , LI, Chaoqun , WEN, Fang , WANG, Wenbo , ZHANG, Hongke , XU, Dan , LI, Chong , SHI, Jie
摘要： Provided in the invention are a catalyst for preparing phosgene and a preparation method therefor, and a method for the preparation of phosgene and the comprehensive utilization of energy thereof. The preparation method comprises the following steps: 1) stirring and soaking activated carbon in a modifying solution, then adding dimethyltin dichloride and chromium oxide powders and carrying out a reaction, and then adding a nickel oxide fine powder and ultrasonically oscillating same to prepare a pre-modified activated carbon; 2) drying the pre-modified activated carbon; and 3) heating and calcinating the dried pre-modified activated carbon from step 2) to prepare the catalyst. Based on the preparation method, thin layers are formed on the surface of the catalyst by bonding chromium tin phosphate and chromium tin silicate with Ni by means of -O-Ni-O-, respectively, which can improve the high-temperature resistance and oxidation resistance of the activated carbon, and improve the safe and stable operation level of a device. The aim of integrated comprehensive utilization of energy is achieved by coupling phosgene production with an evaporation and concentration process of brine and using steam as a heat source for evaporation and concentration of the brine.
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