摘要:
A process is described for the preparation of 2,4-dichlorophenoxyacetic acid consisting of the chlorination of phenoxyacetic acid with chlorine, at temperatures from 0°C to the boiling point of the reaction mixture, in a reaction medium composed of acetic acid.
摘要:
Cadmium is removed from phosphoric acid streams containing it by a process comprising initially treating the stream concerned with halide ions and metallic iron, followed by absorbing the resultant phosphoric solution on adsorption resin not of ion exchange type.
摘要:
A process is disclosed for the preparation of potassium nitrate by means of the reaction of nitric acid with potassium carbonate, wherein potassium carbonate is obtained by means of an electrochemical process.
摘要:
Process for scrubbing by means of a liquid the ammonia contained in a vent (in particular the vents of plants for the synthesis and granulation of urea), wherein said liquid is an aqueous solution of urea neutralized with an acid, the pH of said neutralized solution being from 5.0 to 7.0.
摘要:
Calcium-urea nitrate [Ca(NO₃)₂.4CO(NH₂)₂] is produced by means of a process, according to which: - a liquid composition is prepared, at a temperature not higher than 170°C, which contains urea and calcium nitrate, in a molar ratio to each other equal to, or approximately equal to, 4/1, and having a water content comprised within the range of from 0 to 15% by weight; - said liquid composition is sprayed, through a spray nozzle, on previously formed solid particles of calcium-urea nitrate, kept moving at a temperature comprised within the range of from 40 to approximately 100°C, and under a stream of an inert gas; - calcium-urea nitrate is recovered from said solid products from the spray. The so obtained calcium-urea nitrate is in the form of a granular and free-flowing solid, free from the tendency to form dusts, and is useful in agriculture as a nitrogenous fertilizer. Also the suitable equipment for carrying out the process of calcium-urea nitrate preparation as a continuous process is disclosed.
摘要:
A process is disclosed for the production of water soluble ammonium phosphates, comprising the following steps: a) to react in a reaction step ammonia and untreated phosphoric acid with P 2 0 5 concentration, comprised within the range of from 30 to 54% outcoming from wet processes; b) to filter under high temperature conditions the reaction suspension, separating the impurity-containing sludges from an aqueous solution of ammonium phosphate; c) to cool and crystallize the aqueous solution of ammonium phosphate; d) to separate the formed ammonium phosphate crystals from the mother liquors.
摘要:
A by-pass arrangement for controlling the return flow of a pilot valve is described, which by being connected between the outlet connection from the pilot valve and the return connection to the pilot valve eliminates the return circuit and enables said arrangement to be connected downstream to an open circuit network used for the pulsating delivery of an irrigation liquid.
摘要:
Calcium-urea nitrate [Ca(NO₃)₂.4CO(NH₂)₂] is produced by means of a process, according to which: - a liquid composition is prepared, at a temperature not higher than 170°C, which contains urea and calcium nitrate, in a molar ratio to each other equal to, or approximately equal to, 4/1, and having a water content comprised within the range of from 0 to 15% by weight; - said liquid composition is sprayed, through a spray nozzle, on previously formed solid particles of calcium-urea nitrate, kept moving at a temperature comprised within the range of from 40 to approximately 100°C, and under a stream of an inert gas; - calcium-urea nitrate is recovered from said solid products from the spray. The so obtained calcium-urea nitrate is in the form of a granular and free-flowing solid, free from the tendency to form dusts, and is useful in agriculture as a nitrogenous fertilizer. Also the suitable equipment for carrying out the process of calcium-urea nitrate preparation as a continuous process is disclosed.
摘要:
A continuous process is disclosed for the production, with a high yield, of high purity silicon tetrafluoride, by starting from an aqueous solution of fluosilicic acid, which comprises:
a) the reaction of an aqueous solution of fluosilicic acid with concentrated sulphuric acid, carried out with a short residence time and preferably under fluido-dynamic conditions of turbulence, inside a reaction zone; b) the separation of a gaseous stream containing silicon tetrafluoride from a liquid stream of aqueous sulphuric acid, carried out inside a separation zone, directly connected with the reaction zone; c) the washing, with concentrated and cold sulphuric acid, of said gaseous stream, carried out inside a washing zone, for the purpose of separating a gaseous stream of purified silicon tetrafluoride; and, possibly d) the further purification of said gaseous stream of purified silicon tetrafluoride, by means of techniques of adsorption on an adsorbent solid material.