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1.发明公开MULTIAUTOCLAVE FOR COMBINATORIAL SYNTHESIS OF ZEOLITES AND OTHER MATERIALS 失效MULTIAUTOKLAVE FOR沸石和其他材料的组合的合成
公开(公告)号：EP0968050A1
公开(公告)日：2000-01-05
申请号：EP98904447.4
申请日：1998-02-20
申请人： SINVENT A/S
CPC分类号： B01J3/04 , B01J19/0046 , B01J2219/00313 , B01J2219/00319 , B01J2219/00335 , B01J2219/00349 , B01J2219/00477 , B01J2219/00585 , B01J2219/00596 , B01J2219/00601 , B01J2219/00745 , B01J2219/00747 , B01J2219/00754 , C01B39/02 , C40B30/08 , C40B40/18 , C40B60/14
摘要： The invention relates to a multiautoclave and details of its design and a method for automated synthesis of zeolites in said multiautoclave and, furthermore, application of the multiautoclave for an automated synthesis which is optimized simultaneously with regard to several synthesis parameters in the synthesis of zeolites. The multiautoclave consists typically of a pressure vessel/autoclave lined with an inert material with from 10 to 10.000 small, separated chambers, each typically having a volume of 0,2-2 ml, the chambers preferably being formed as through-going perforations in a central block and the perforations are sealed by means of balls, septa, stoppers or such which are placed at the bottom and top of each through-going perforation, and metal plates are placed over and under the Teflon plate so that the closing mechanism is pressed against the edges of the perforations in the Teflon plate with sufficient load to enable the chambers to be filled with aqueous mixtures and to be heated to 200 °C without the occurence of leakage. Top-and bottom plates and closing mechanisms can be integrated so that all the perforations are sealed simultaneously when these are placed at the top and bottom sides of the central block.
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2.发明授权MULTIAUTOCLAVE FOR COMBINATORIAL SYNTHESIS OF ZEOLITES AND OTHER MATERIALS 失效MULTIAUTOKLAVE FOR沸石和其他材料的组合的合成
公开(公告)号：EP0968050B1
公开(公告)日：2001-09-26
申请号：EP98904447.4
申请日：1998-02-20
申请人： SINVENT A/S
CPC分类号： B01J3/04 , B01J19/0046 , B01J2219/00313 , B01J2219/00319 , B01J2219/00335 , B01J2219/00349 , B01J2219/00477 , B01J2219/00585 , B01J2219/00596 , B01J2219/00601 , B01J2219/00745 , B01J2219/00747 , B01J2219/00754 , C01B39/02 , C40B30/08 , C40B40/18 , C40B60/14
摘要： The invention relates to a multiautoclave and details of its design and a method for automated synthesis of zeolites in said multiautoclave and, furthermore, application of the multiautoclave for an automated synthesis which is optimized simultaneously with regard to several synthesis parameters in the synthesis of zeolites. The multiautoclave consists typically of a pressure vessel/autoclave lined with an inert material with from 10 to 10.000 small, separated chambers, each typically having a volume of 0,2-2 ml, the chambers preferably being formed as through-going perforations in a central block and the perforations are sealed by means of balls, septa, stoppers or such which are placed at the bottom and top of each through-going perforation, and metal plates are placed over and under the Teflon plate so that the closing mechanism is pressed against the edges of the perforations in the Teflon plate with sufficient load to enable the chambers to be filled with aqueous mixtures and to be heated to 200 DEG C without the occurence of leakage. Top-and bottom plates and closing mechanisms can be integrated so that all the perforations are sealed simultaneously when these are placed at the top and bottom sides of the central block.
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