摘要:
Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of forming a cyclic sulfur trioxide adduct; hydrolyzing the cyclic sulfur trioxide adduct to form an acesulfame-H composition comprising acesulfame-H; neutralizing the acesulfame-H in the acesulfame-H composition to form a crude acesulfame potassium composition comprising acesulfame potassium and less than 2800 wppm acetoacetamide-N-sulfonic acid, wherein the neutralizing step is conducted or maintained at a pH at or below 11.0; and treating the crude acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 37 wppm acetoacetamide-N-sulfonic acid.
摘要:
High purity acesulfame potassium obtained by an improved process. In one embodiment, the process comprises the steps of contacting a solvent, e.g., dichloromethane, and a cyclizing agent, e.g., sulfur trioxide, to form a cyclizing agent composition and reacting an acetoacetamide salt with the cyclizing agent in the composition to form a cyclic sulfur trioxide adduct. The contact time is less than 60 minutes. The process also comprises forming from the cyclic sulfur trioxide adduct composition a finished acesulfame potassium composition comprising non-chlorinated, e.g., non-chlorinated, acesulfame potassium and less than 35 wppm 5-halo acesulfame potassium, preferably less than 5 wppm.
摘要:
Improved processes for producing high purity acesulfame potassium. In one embodiment, the process comprises the steps of contacting a solvent, e.g., dichloromethane, and a cyclizing agent, e.g., sulfur trioxide, to form a cyclizing agent composition and reacting an acetoacetamide salt with the cyclizing agent in the composition to form a cyclic sulfur trioxide adduct. The contact time is less than 60 minutes. The process also comprises forming from the cyclic sulfur trioxide adduct composition a finished acesulfame potassium composition comprising non-chlorinated, e.g., non-chlorinated, acesulfame potassium and less than 35 wppm 5-halo acesulfame potassium, preferably less than 5 wppm.
摘要:
The invention relates to a method for producing a sweetener salt of formula APMH+Ace-, according to which aspartame or an aspartame derivative is reacted with acesulfamic acid in a solvent selected among one or several of the following: liquid SO2, halogenated aliphatic hydrocarbons, carbonic acid esters comprising low, aliphatic alcohols, nitroalkanes, alkyl-substituted pyridines, aliphatic sulfones. The invention also relates to the use of said sweetener salts in food, beverages, pharmaceuticals, and cosmetics.
摘要:
Komplexe Verbindungen enthaltend Acesulfam besitzen eine gute antimikrobielle Wirkung, insbesondere antibakterielle Wirkung und zeichnen sich dadurch aus, dass sie Komplexverbindungen von metallischen Elementen wie Zink, Kupfer, Silber oder nichtmetallischen quartären Ammoniumkationen, wie dem Cetylpyridiniumkation, mit Acesulfam sind. Die Erfindung betrifft auch ein Verfahren zum Herstellen der Verbindungen und deren Verwendung im Bereich der Mundhygiene.
摘要:
Die Erfindung betrifft eine Verbindung enthaltend ein Nichtmetallkation und ein Acesulfamanion, wobei gegebenenfalls zusätzlich Kristallwasser vorhanden sein kann. Als Nichtmetallkation enthält die Verbindung vorzugsweise ein Ammoniumkation. Die Erfindung betrifft auch ein Verfahren zur Herstellung der erfindungsgemäßen Verbindung und ihre Verwendung zum Süßen von Nahrungsmitteln und Getränken.