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    Method for producing epoxy compound
    36.
    发明专利
    Method for producing epoxy compound 有权
    生产环氧化合物的方法

    公开(公告)号：JP2013241376A

    公开(公告)日：2013-12-05

    申请号：JP2012116391

    申请日：2012-05-22

    申请人： Jx Nippon Oil & Energy Corp ,  Jx日鉱日石エネルギー株式会社 ,  Osaka Univ ,  国立大学法人大阪大学

    发明人： ICHIHARA JUNKO ,  YAMAGUCHI TOSHIRO ,  KAMEYAMA ATSUSHI ,  SUZUKI TAKASHI ,  MORIKITA TAKASHI

    IPC分类号： C07D301/12 ,  C07D493/04

    CPC分类号： C07D301/12 ,  C07D493/04

    摘要： PROBLEM TO BE SOLVED: To provide a method for epoxidating an olefin compound highly productively.SOLUTION: A method for producing an epoxy compound by reacting a compound having a carbon-carbon double bond with hydrogen peroxide includes the following steps repeatedly or continuously. Step (1): reacting a compound having a carbon-carbon double bond and hydrogen peroxide in the coexistence of (a) the compound having a carbon-carbon double bond, (b) the hydrogen peroxide solution, (c) a solid carrier powder, and (d) a solid catalyst powder, or further (e) an organic solvent. Step (2): separating an epoxy compound from the reaction mixture of the step (1). Step (3): adding (d) the solid catalyst powder, and adding (a) the compound having a carbon-carbon double bond and (b) the hydrogen peroxide solution, or further (e) the organic solvent to a powder mixture composed of the solid carrier and the solid catalyst after the reaction product has been separated in the step (2).

    摘要翻译： 要解决的问题：提供一种高效地环氧化烯烃化合物的方法。解决方案：通过使具有碳 - 碳双键的化合物与过氧化氢反应制备环氧化合物的方法包括重复或连续地进行以下步骤。 步骤（1）：在（a）具有碳 - 碳双键的化合物，（b）过氧化氢溶液，（c）固体载体粉末（a）中，使具有碳 - 碳双键的化合物和过氧化氢 ，和（d）固体催化剂粉末，或进一步（e）有机溶剂。 步骤（2）：从步骤（1）的反应混合物中分离环氧化合物。 步骤（3）：加入（d）固体催化剂粉末，并将（a）具有碳 - 碳双键的化合物和（b）过氧化氢溶液，或（e）有机溶剂加入到由 的固体载体和固体催化剂在步骤（2）中已经分离出反应产物之后。

    Method of manufacturing an epoxy compound
    37.
    发明专利
    Method of manufacturing an epoxy compound 有权

    公开(公告)号：JP5294771B2

    公开(公告)日：2013-09-18

    申请号：JP2008238787

    申请日：2008-09-18

    申请人： 日本化薬株式会社

    发明人： 政隆 中西 ,  健一 窪木 ,  直房 宮川

    IPC分类号： C07D301/12 ,  C07B61/00 ,  C07D301/32 ,  C07D303/44

    摘要： PROBLEM TO BE SOLVED: To provide a high-purity epoxy compound containing little amount of a residual catalyst. SOLUTION: The production method of the epoxy compound comprises subjecting a compound having a carbon-carbon double bond to an oxidation reaction in the presence of hydrogen peroxide, a quaternary ammonium salt and a heteropolyacid and subsequently removing the quaternary ammonium salt remaining in the reaction mixture by a chemical-activated carbon. COPYRIGHT: (C)2010,JPO&INPIT

    Method for producing multivalent glycidyl compound
    39.
    发明专利
    Method for producing multivalent glycidyl compound 有权
    生产多糖甘油化合物的方法

    公开(公告)号：JP2013112649A

    公开(公告)日：2013-06-10

    申请号：JP2011260922

    申请日：2011-11-29

    申请人： Showa Denko Kk ,  昭和電工株式会社

    发明人： MIYASAKA RYUTA ,  ISHIBASHI KEITAKA ,  FUKUMOTO NAOYA ,  UCHIDA HIROSHI

    IPC分类号： C07D303/30 ,  C07D301/12

    摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently producing a multivalent glycidyl compound by oxidizing a multivalent allyl compound by the use of an aqueous solution of hydrogen peroxide as an oxidizing agent.SOLUTION: The method includes a step of using a multivalent allyl compound possessing three or more allyl groups as a substrate, a step of interrupting the reaction on the way of the epoxidation reaction and removing water in the reaction liquid, and a step of thereafter conducting the epoxidation reaction again. The hydrolysis of the glycidyl group of the reaction intermediate generated along with the course of the reaction is suppressed by removing water in the reaction liquid on the way of the reaction. Preferably the reaction is conducted in the presence of acetonitrile and alcohol.

    摘要翻译： 待解决的问题：提供通过使用过氧化氢水溶液作为氧化剂氧化多价烯丙基化合物来有效制备多价缩水甘油基化合物的方法。 解决方案：该方法包括使用具有三个或更多个烯丙基的多价烯丙基化合物作为底物的步骤，在环氧化反应途中中断反应并除去反应液中的水的步骤，以及步骤 之后再次进行环氧化反应。 与反应过程一起产生的反应中间体的缩水甘油基的水解通过在反应途中除去反应液中的水来抑制。 反应优选在乙腈和乙醇的存在下进行。 版权所有（C）2013，JPO＆INPIT

    Quaternary ammonium salt, catalyst for oxidation reaction containing the same, method for producing epoxy compound, and method for separating the catalyst for oxidation reaction
    40.
    发明专利
    Quaternary ammonium salt, catalyst for oxidation reaction containing the same, method for producing epoxy compound, and method for separating the catalyst for oxidation reaction 审中-公开
    季铵盐，含氧化反应的催化剂，环氧化合物的制造方法，以及用于分离催化剂进行氧化反应的方法

    公开(公告)号：JP2013112639A

    公开(公告)日：2013-06-10

    申请号：JP2011260212

    申请日：2011-11-29

    申请人： Daicel Corp ,  株式会社ダイセル

    发明人： SUZUKI TAKAMASA ,  TAKASE ICHIRO

    IPC分类号： C07C217/08 ,  B01J31/34 ,  C07B61/00 ,  C07D301/12 ,  C07D303/04

    CPC分类号： Y02P20/52

    摘要： PROBLEM TO BE SOLVED: To provide a quaternary ammonium salt capable of separating simply and easily a catalyst for oxidation reaction from a product in a reaction solution after reaction, in a method for producing the oxidized product by oxidizing an organic compound with hydrogen peroxide in the presence of the catalyst for the oxidation reaction.SOLUTION: There is disclosed a quaternary ammonium salt expressed by formula (1), wherein R, R, Reach independently represents a hydrocarbon group which may have a substituent; R4 represents a hydrogen atom or a hydrocarbon group which may have a substituent; Xrepresents a counter anion; and n is an integer of 1-20.

    摘要翻译： 待解决的问题：提供能够简单且容易地从反应后的反应溶液中的产物分离氧化反应催化剂的季铵盐，在通过用氢气氧化有机化合物的方法中生产氧化产物 在催化剂存在下进行氧化反应。 解决方案：公开了由式（1）表示的季铵盐，其中R 1 ，R 2 各自独立地表示可以具有取代基的烃基; R4表示氢原子或可具有取代基的烃基; -X - 表示抗衡阴离子; n为1-20的整数。 版权所有（C）2013，JPO＆INPIT