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    바이나프톨 알데히드 유도체 및 그의 중간체의 제조방법
    1.
    发明公开
    바이나프톨 알데히드 유도체 및 그의 중간체의 제조방법 有权
    制备二氢萘二甲酸衍生物及其中间体的方法

    公开(公告)号：KR1020100054628A

    公开(公告)日：2010-05-25

    申请号：KR1020080113616

    申请日：2008-11-14

    Applicant: 주식회사 아미노룩스

    Inventor： 김관묵 ,  안윤수 ,  박현정

    IPC: C07C45/27 ,  C07C49/487 ,  C07C49/497

    CPC classification number: C07C45/27 ,  C07C49/487

    Abstract: PURPOSE: A producing method of a binaphthol aldehyde derivative is provided to increase the selectivity for a hydrogen position of a 2,2'-binaphthol-3-aldehyde 2` hydroxy group, and to produce the binaphthol aldehyde derivative without generating by-products. CONSTITUTION: A producing method of a binaphthol aldehyde derivative marked as chemical formula 1 comprises the following steps: reducing a compound marked as chemical formula 3 to obtain a compound marked as chemical formula 2; and oxidizing the compound marked as the chemical formula 2. In the chemical formula 1~3, X is selected from the group consisting of hydrogen, halogen, amino, nitro, cyano, formyl, carboxyl, substituted or non-substituted alkyl of C1~C10, alkylcarbonyl of C1~C10, aryl of C6~C10, and alkoxy of C1~C10. N and M are integers of 0~5.

    Abstract translation: 目的：提供联萘酚醛衍生物的制备方法以增加对2,2'-联萘酚-3-醛2'羟基的氢位的选择性，并产生不产生副产物的联苯酚醛衍生物。 构成：标记为化学式1的联萘酚醛衍生物的制备方法包括以下步骤：还原标记为化学式3的化合物，得到标记为化学式2的化合物; 在化学式1〜3中，X选自氢，卤素，氨基，硝基，氰基，甲酰基，羧基，取代或未取代的C1〜 C10，C1〜C10的烷基羰基，C6〜C10的芳基，C1〜C10的烷氧基。 N和M是0〜5的整数。

    바이나프톨 알데히드 유도체 및 그의 제조방법
    2.
    发明授权
    바이나프톨 알데히드 유도체 및 그의 제조방법 有权
    联萘醛衍生物及其制备方法

    公开(公告)号：KR101087498B1

    公开(公告)日：2011-11-28

    申请号：KR1020080113614

    申请日：2008-11-14

    Applicant: 주식회사 아미노룩스

    Inventor： 김관묵 ,  안윤수 ,  박현정

    IPC: C07C39/23

    CPC classification number: C07C45/71 ,  C07C47/575 ,  C07C67/343 ,  C07C69/94

    Abstract: 본 발명은 하기 화학식 1의 화합물 및 그의 제조방법에 관한 것이다.
    [화학식 1]

    상기 화학식 1의 화합물은 2,2'-바이나프톨-3-알데히드의 2' 히드록시기의 수소 위치에 다양한 치환기를 매우 효율적으로 도입하는 것을 가능하게 한다. 또한, 본 발명의 제조방법은 상기 화학식 1의 화합물을 매우 안전한 방법으로 저렴하게 제조하는 방법을 제공한다.
    키랄 합성, 아미노산, 아미노 알코올, 바이나프톨

    광학적으로 순수한 아미노산을 얻는 방법
    4.
    发明公开
    광학적으로 순수한 아미노산을 얻는 방법 有权
    获得光稳定氨基酸的方法

    公开(公告)号：KR1020100106221A

    公开(公告)日：2010-10-01

    申请号：KR1020100024590

    申请日：2010-03-19

    Applicant: 주식회사 아미노룩스

    Inventor： 김관묵 ,  김호준

    IPC: C07C273/16 ,  C07C275/38 ,  C07B57/00 ,  C07B55/00

    CPC classification number: C07C273/16 ,  C07B55/00 ,  C07B57/00 ,  C07B2200/07 ,  C07C227/34 ,  C07C227/36 ,  C07C319/28 ,  C07D209/20 ,  C07C275/32 ,  C07C229/36 ,  C07C229/22 ,  C07C229/08 ,  C07C323/58

    Abstract: PURPOSE: An obtaining method of optically pure amino acid is provided to remarkably reduce the optics conversion time, and to economically mass produce the amino acid with a simple manufacturing process. CONSTITUTION: An obtaining method of optically pure amino acid comprises the following steps: mixing a basic solution including amino acid for the optical separation or the optical conversion, and an organic solution including a chiral selective acceptor forming imine by selectively chiral-reacting with D-type or L-type amino acid, and separating a basic solution layer, and an organic solution layer; mixing the organic solution with an aqueous acidic solution, and separating an aqueous acidic solution layer and the organic solution layer; and obtaining the D-type or L-type amino acid form the aqueous acidic solution.

    Abstract translation: 目的：提供光学纯氨基酸的获得方法，显着降低光学转化时间，并以简单的制造工艺经济地大量生产氨基酸。 构成：光学纯氨基酸的获得方法包括以下步骤：将包含用于光学分离或光学转换的氨基酸的碱性溶液与包含手性选择性受体形成亚胺的有机溶液混合，通过选择性地与D- 型或L型氨基酸，并分离碱性溶液层和有机溶液层; 将有机溶液与酸性水溶液混合，分离酸性水溶液层和有机溶液层; 得到酸性水溶液形成的D型或L型氨基酸。

    바이나프톨 알데히드 유도체 및 그의 제조방법
    5.
    发明公开
    바이나프톨 알데히드 유도체 및 그의 제조방법 有权
    二萘基醚衍生物及其制备方法

    公开(公告)号：KR1020100054627A

    公开(公告)日：2010-05-25

    申请号：KR1020080113614

    申请日：2008-11-14

    Applicant: 주식회사 아미노룩스

    Inventor： 김관묵 ,  안윤수 ,  박현정

    IPC: C07C39/23

    CPC classification number: C07C45/71 ,  C07C47/575 ,  C07C67/343 ,  C07C69/94

    Abstract: PURPOSE: A binaphthol aldehyde derivative and a producing method thereof are provided to safely produce the binaphthol aldehyde derivative without using dangerous materials including n-butyl lithium. CONSTITUTION: A binaphthol aldehyde derivative is marked as chemical formula 1. In the chemical formula 1, X refers to an alkyl group of C1~C10 substituted with more than one substituent selected from the group consisting of hydrogen, halogen, amino, nitro, cyano, formyl, carboxyl, halogen, hydroxyl, and aryl of C6~C10, alkylcarbonyl of C1~C10, and alkoxy of C1~C10, respectively. N and M are integers of 0~5. R1 is selected from the group consisting of the alkyl of C1~C5, arylalkyl of C6~C10 and alkoxy alkyl of C2~C10.

    Abstract translation: 目的：提供联萘酚醛衍生物及其制备方法，以安全生产该萘酚醛衍生物，而不使用包括正丁基锂在内的危险物质。 构成：联萘酚醛衍生物被标记为化学式1.在化学式1中，X是指被多个选自氢，卤素，氨基，硝基，氰基的取代基取代的C1〜C10的烷基 ，甲酰基，羧基，卤素，羟基和C6〜C10的芳基，C1〜C10的烷基羰基和C1〜C10的烷氧基。 N和M是0〜5的整数。 R1选自C1〜C5的烷基，C6〜C10的芳基烷基和C2〜C10的烷氧基烷基。

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