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    이차 알코올의 라세미화 또는 동적속도론적 광학분할에 유용한 루테늄 촉매
    2.
    发明公开
    이차 알코올의 라세미화 또는 동적속도론적 광학분할에 유용한 루테늄 촉매 失效
    用于二次醇的动力学动力学分析中使用的钌催化剂

    公开(公告)号：KR1020090037211A

    公开(公告)日：2009-04-15

    申请号：KR1020070102738

    申请日：2007-10-11

    Applicant: 포항공과대학교 산학협력단

    Inventor： 박재욱 ,  김남두 ,  김만주 ,  고수병

    IPC: C07F15/00

    CPC classification number: C07F15/0046 ,  B01J31/1616 ,  B01J2531/821 ,  C07C67/293

    Abstract: A ruthenium catalyst is provided to be synthesized simply at high yield, and to perform racemization or dynamic kinetic resolution of secondary alcohols at room temperature in atmosphere stably. A ruthenium complex compound is represented by the chemical formula 1. In the chemical formula 1, R1 and R2 are independently hydrogen or substituted or unsubstituted phenyl, C1-5 alkyl, C2-5 alkenyl or C2-5 alkynyl; R3 is - C (O) -R4 or -Si-R5; R4 is C1-10 alkyl, C3-10 aryl, C1-10 alkoxy or substituted or unsubstituted phenyl; R5 is C1-10 alkyl or C3-10 aryl; X is halogen; and Y and Z are independently hydrogen, carbonyl or phosphine.

    Abstract translation: 提供钌催化剂以简单地高收率合成，并稳定地在室温下进行仲醇的外消旋化或动态动力学拆分。 钌配位化合物由化学式1表示。在化学式1中，R 1和R 2独立地为氢或取代或未取代的苯基，C 1-5烷基，C 2-5烯基或C 2-5炔基; R3是-C（O）-R4或-Si-R5; R4是C1-10烷基，C3-10芳基，C1-10烷氧基或取代或未取代的苯基; R5是C1-10烷基或C3-10芳基; X是卤素; Y和Z独立地为氢，羰基或膦。

    노보넨 단량체 조성물의 제조 방법, 이로부터 제조되는노보넨 중합체, 상기 노보넨 중합체를 포함하는 광학 필름,및 상기 노보넨 중합체의 제조 방법
    3.
    发明公开
    노보넨 단량체 조성물의 제조 방법, 이로부터 제조되는노보넨 중합체, 상기 노보넨 중합체를 포함하는 광학 필름,및 상기 노보넨 중합체의 제조 방법 有权
    制备异腈单体组合物的方法，由其制备的NORBNENENE聚合物，包含NORBENNENE聚合物的光学膜和制备NORBENNENE聚合物的方法

    公开(公告)号：KR1020080007426A

    公开(公告)日：2008-01-21

    申请号：KR1020077018203

    申请日：2007-06-26

    Applicant: 주식회사 엘지화학

    Inventor： 최대승 ,  정혜영 ,  홍성돈 ,  이정민 ,  이희진 ,  전성호

    IPC: C07C69/74 ,  C08F32/00 ,  C08J5/18 ,  G02F1/1335

    CPC classification number: C08F32/08 ,  C07C67/293 ,  C07C2602/42 ,  Y10T428/10 ,  Y10T428/1086 ,  C07C69/007 ,  C07C69/145

    Abstract: A method for preparing a norbornene monomer composition is provided to obtain a high exo-isomer content by controlling reaction temperature, reaction time, molar ratio of reactants and addition of a solvent while not adding a catalyst. A method for preparing a norbornene monomer composition comprises a step of reacting cyclopentadiene, dicyclopentadiene or a mixture thereof, a compound represented by the formula of CH2=CH-(CH2)n-OC(O)R (wherein n is an integer of 0-10, and R is a C1-C20 alkyl group) at a reaction temperature of 230-330 deg.C for a reaction time of 5 minutes-24 hours to obtain an exo-isomer content of at least 50 mol%. The compound represented by the formula is used in a molar ratio of 1:1-1:10 based on the cyclopentadiene, dicyclopentadiene or a mixture thereof.

    Abstract translation: 提供制备降冰片烯单体组合物的方法，通过控制反应温度，反应时间，反应物的摩尔比和加入溶剂而不添加催化剂来获得高的外异构体含量。 制备降冰片烯单体组合物的方法包括使环戊二烯，二环戊二烯或其混合物，由CH 2 = CH-（CH 2）n -OC（O）R（其中n为整数0）表示的化合物 -10，R为C1-C20烷基），反应温度为230-330℃，反应时间为5分钟至24小时，得到至少50摩尔％的外异构体含量。 由式表示的化合物以基于环戊二烯，二环戊二烯或其混合物的摩尔比为1：1-1：10使用。

    1-아세톡시-3-(3,4-C1 또는 C2알킬렌디옥시페닐) 프로펜 화합물
    5.
    发明公开
    1-아세톡시-3-(3,4-C1 또는 C2알킬렌디옥시페닐) 프로펜 화합물 失效
    1-乙酰基-3-（取代苯基）丙酸

    公开(公告)号：KR1020050088255A

    公开(公告)日：2005-09-02

    申请号：KR1020057013591

    申请日：2003-12-18

    Applicant: 우베 고산 가부시키가이샤

    Inventor： 시라이마사시 ,  요시다요시히로 ,  사다이케신이치로

    IPC: C07C69/157 ,  C07C67/293

    CPC classification number: C07D317/54 ,  C07C67/293 ,  C07C69/007 ,  C07D319/18 ,  C07C69/157

    Abstract: Compounds represented by the general formula (I) can be produced by reacting a benzene compound represented by the general formula (IV) or (V) with an alkenylidene diacetate represented by the general formula (VI) in the presence of a catalyst comprising (a) a boron halide, (b) a triflate of a group 11 element, (c) a halide of a group 12 element, and (d) at least one member selected from among triflates and halides of tin and elements of atomic numbers of 58 and 66 to 71: (I) (IV) (V) (VI) wherein R1 and R2 are each H or C1-10 alkyl; A is a substituted phenyl group corresponding to a compound of the general formula (IV) or (V); R 3 and R4 are each C1-4 alkyl; m is 0 or 1 to 4; n is 1 to 5; and k is 1 or 2.

    Abstract translation: 由通式（I）表示的化合物可以通过使由通式（IV）或（V）表示的苯化合物与由通式（VI）表示的亚烯基二乙酸酯在催化剂存在下反应来制备，所述催化剂包含（a ）卤化硼，（b）11族元素​​的三氟甲磺酸酯，（c）第12族元素的卤化物，和（d）选自锡的三氟甲磺酸酯和卤化物中的至少一种，原子数为58的元素 和66至71：（I）（IV）（V）（VI）其中R 1和R 2各自为H或C 1-10烷基; A是对应于通式（IV）或（V）化合物的取代苯基; R 3和R 4各自为C 1-4烷基; m为0或1〜4; n为1至5; k为1或2。

    메틸포르메이트이성질화에의한아세트산및/또는메틸아세테이트의제조방법
    6.
    发明公开
    메틸포르메이트이성질화에의한아세트산및/또는메틸아세테이트의제조방법 失效
    通过甲基异构化生产乙酸和/或乙酸甲酯的方法

    公开(公告)号：KR1020000004968A

    公开(公告)日：2000-01-25

    申请号：KR1019980707572

    申请日：1997-03-27

    Applicant: 아쓰떽스 쉬미

    Inventor： 빠뚜와꺄를 ,  뻬롱로베르 ,  띠에보다니엘

    IPC: C07C53/08 ,  C07C51/353 ,  C07C67/293 ,  C07C69/14

    CPC classification number: C07C51/353 ,  C07C67/293 ,  C07C53/08 ,  C07C69/14

    Abstract: PURPOSE: A new method using isomerization reaction in the presence of strong acid is proposed to obtain substantial industrial profits. The method somewhat contributes to the enhancement of the reaction activity, but should use additional compound thus cannot be simplified. CONSTITUTION: A producing method of the invention is performed in the presence of catalyst system including methyl formate, water, solvent and 1 or more halogenation accelerator and 1 or more Ir compound. The method maintains the partial pressure of CO somewhat constantly during the reaction and maintains the amount of polyformate less than 20wt% of reacting medium.

    Abstract translation: 目的：提出在强酸存在下使用异构化反应的新方法，以获得实质性的工业利润。 该方法有助于提高反应活性，但应使用其他化合物，因此不能简化。 构成：本发明的制备方法在包括甲酸甲酯，水，溶剂和1种或更多种卤化促进剂和1种或更多种Ir化合物的催化剂体系的存在下进行。 该方法在反应过程中保持CO的分压一定程度，并保持聚甲酸酯的量少于反应介质的20wt％。

    폴리플루오로알킬알릴 화합물 및 그 제조법
    7.
    发明公开
    폴리플루오로알킬알릴 화합물 및 그 제조법 审中-实审
    多氟烷基烯丙基化合物及其制备方法

    公开(公告)号：KR1020170063654A

    公开(公告)日：2017-06-08

    申请号：KR1020177008742

    申请日：2015-09-18

    Applicant: 유니마테크 가부시키가이샤

    Inventor： 후쿠시마타케시

    IPC: C07C21/18 ,  C07C17/361 ,  C07C69/14 ,  C07C67/293

    CPC classification number: C07C21/18 ,  C07C17/361 ,  C07C17/363 ,  C07C67/293 ,  C07C69/14 ,  C07C69/63

    Abstract: 일반식 CF(CF)(CHCF)(CFCF)CHCH=CH[I] (n: 0∼5, a: 1 또는 2, b: 0∼3)로표시되는폴리플루오로알킬알릴화합물. 이폴리플루오로알킬알릴화합물은, 일반식 CF(CF)(CHCF)(CFCF)CHCHICHOCOR' [II] (n, a, b: 상기정의와동일함, R': 탄소수 1∼3의알킬기)로표시되는카복실산알릴부가체에천이금속을반응시킴으로써제조된다. 이제조법에서는, 환경부하가높은금속시약을사용하지않아, 하이드로실릴화반응을행하기전에원료화합물유래의유리아이오딘을제거하는것이가능하며, 또한핸들링성도양호한함불소알킬실레인화합물의합성중간체로서사용되는폴리플루오로알킬알릴화합물을제공한다.

    Abstract translation: 式CF（CF）（CHCF）（CFCF）CHCH = CH [I]（n为0〜5，：1或2，B：0〜3）由多氟烷表示烷基烯丙基化合物。 与多氟烷烷基烯丙基化合物是由通式CF（CF）（CHCF）（CFCF）CHCHICHOCOR表示 '[II]（N，A，B：与上述相同的定义，R'：具有1至3个碳原子数的烷基） 与过渡金属反应至指定的羧酸烯丙基加合物。 现在逐项，不使用环境负荷高的金属试剂，进行能够消除从起始化合物衍生的游离碘，并且还处理成都优选氟化烷基硅烷的合成中间体的化合物的前的氢化硅烷化反应 L t;多氟烷基烯丙基。

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