公开(公告)号：US09255069B2

公开(公告)日：2016-02-09

申请号：US14084888

申请日：2013-11-20

Applicant: BASF SE

Inventor： Rolf Pinkos ,  Thomas Vogler ,  Karl Ott

IPC: C07D207/267 ,  C07D207/273 ,  C07D207/263

CPC classification number: H01M4/139 ,  C07D207/263 ,  C07D207/273 ,  H01M4/04

Abstract: Process for purifying N-alkylpyrrolidones which due to a previous use comprise at least one of the impurities of the formula I or II where R is hydrogen or a C1-C20-alkyl group, wherein a basic compound is added to the N-alkylpyrrolidone to be purified and the temperature of the mixture is at least 80° C. not more than 20 minutes after addition of the basic compound and N-alkylpyrrolidone is distilled off from the mixture obtained.

Abstract translation: 由于先前使用而提纯N-烷基吡咯烷酮的方法包括至少一种式I或II的杂质，其中R是氢或C1-C20烷基，其中将碱性化合物加到N-烷基吡咯烷酮中 纯化，混合物的温度至少为80℃，加入碱性化合物后不超过20分钟，从得到的混合物中蒸馏除去N-烷基吡咯烷酮。

公开(公告)号：US20140142323A1

公开(公告)日：2014-05-22

申请号：US14084888

申请日：2013-11-20

Applicant: BASF SE

Inventor： Rolf Pinkos ,  Thomas Vogler ,  Karl Ott

IPC: C07D207/273

CPC classification number: H01M4/139 ,  C07D207/263 ,  C07D207/273 ,  H01M4/04

Abstract: Process for purifying N-alkylpyrrolidones which due to a previous use comprise at least one of the impurities of the formula I or II where R is hydrogen or a C1-C20-alkyl group, wherein a basic compound is added to the N-alkylpyrrolidone to be purified and the temperature of the mixture is at least 80° C. not more than 20 minutes after addition of the basic compound and N-alkylpyrrolidone is distilled off from the mixture obtained.

Abstract translation: 由于先前使用而提纯N-烷基吡咯烷酮的方法包括至少一种式I或II的杂质，其中R是氢或C1-C20烷基，其中将碱性化合物加到N-烷基吡咯烷酮中 纯化，混合物的温度至少为80℃，加入碱性化合物后不超过20分钟，从得到的混合物中蒸馏除去N-烷基吡咯烷酮。

公开(公告)号：US09923194B2

公开(公告)日：2018-03-20

申请号：US15017864

申请日：2016-02-08

Applicant: BASF SE

Inventor： Rolf Pinkos ,  Thomas Vogler ,  Karl Ott

IPC: C07D201/16 ,  C07D207/267 ,  H01M4/04 ,  H01M4/139 ,  C07D207/273 ,  C07D207/263

CPC classification number: H01M4/139 ,  C07D207/263 ,  C07D207/273 ,  H01M4/04

Abstract: Process for purifying N-alkylpyrrolidones which due to a previous use comprise at least one of the impurities of the formula I or II where R is hydrogen or a C1-C20-alkyl group, wherein a basic compound is added to the N-alkylpyrrolidone to be purified and the temperature of the mixture is at least 80° C. not more than 20 minutes after addition of the basic compound and N-alkylpyrrolidone is distilled off from the mixture obtained.